Preparation and characterization of PTFE coating in new polymer quartz piezoelectric crystal sensor for testing liquor products

doi:10.1088/1674-1056/24/7/078106

Abstract A new method was developed based on the electron beam vacuum dispersion (EBVD) technology to prepare the PTFE polymer coating of the new polymer quartz piezoelectric crystal sensor for testing liquor products. The new method was applied in the new EBVD equipment which we designed. A real-time system monitoring the polymer coating's thickness was designed for the new EBVD equipment according to the quartz crystal microbalance (QCM) principle, playing an important role in preparing stable and uniform PTFE polymer coatings of the same thickness. 30 pieces of PTFE polymer coatings on the surface of the quartz crystal basis were prepared with the PTFE polymer ultrafine powder (purity ≥ 99.99%) as the starting material. We obtained 30 pieces of new PTFE polymer sensors. By using scanning electron microscopy (SEM), the structure of the PTFE polymer coating's column clusters was studied. One sample from the 30 pieces of new PTFE polymer sensors was analysed by SEM in four scales, i.e., 400×, 1000×, 10000×, and 25000×. It was shown that under the condition of high bias voltage and low bias current, uniformly PTFE polymer coating could be achieved, which indicates that the new EBVD equipment is suitable for mass production of stable and uniform polymer coating.

Keywords: PTFE coating electron beam vacuum dispersion mass production of polymer coating

Received: 17 December 2014
Revised: 20 January 2015
Accepted manuscript online:

PACS:	81.15.-z	(Methods of deposition of films and coatings; film growth and epitaxy)
	81.15.Rs	(Spray coating techniques)
	68.55.-a	(Thin film structure and morphology)

Fund: Project supported by the National High Technology Research and Development Program of China (Grant No. 2013AA030901).

Corresponding Authors: Gu Yu
E-mail: guyu@ustb.edu.cn

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Gu Yu (谷宇), Li Qiang (李强) Preparation and characterization of PTFE coating in new polymer quartz piezoelectric crystal sensor for testing liquor products 2015 Chin. Phys. B 24 078106

[1]	Gu Y, Lu Q, Tian F F and Xu B J 2013 Chin. Phys. Lett. 30 108101
[2]	Gu Y, Lu Q, Xu B J and Zhao Z 2013 Chin. Phys. B 23 017804
[3]	Gu Y, Li Q, Tian F F and Xu B J 2013 Lecture Notes in Electrical Engineering 293 121
[4]	Turyan I and Mandler D 1998 J. Am. Chem. Soc. 120 10711
[5]	Ulman A 1996 Chem. Rev. 96 1533
[6]	Decher G, Hong J D and Schmitt J 1992 Thin Solid Films 201-211 831
[7]	Ding S J, Wang P F, Zhang W, Wang J T, Lee W W, Zhang Y W and Xia Z F 2000 Chin. Phys. 9 0778
[8]	Watcharotone S, Dikin D A, Stankovich S, Piner R, Jung I, Dommett G H B, Evmenenko G, Wu S E, Chen S F, Liu C P, Nguyen S T and Ruoff R S 2007 Nano Lett. 7 1888
[9]	Blake P, Brimicombe P D, NAIR R R, Booth T J, Jiang D, Schedin F, Ponomarenko L A, Morozov S V, Gleeson H F, Hill E W, Geim A K and Novoselov K S 2008 Nano Lett. 8 1704
[10]	Wang S J, Geng Y, Zheng Q B and Kim J K 2010 Carbon 48 1815
[11]	Zheng Q B, Gudarzi M M, Wang S J, Geng Y, LI Z G and Kim J K 2011 Carbon 49 2905
[12]	Wang X, Zhi L J and Mullen K 2008 Nano Lett. 8 323
[13]	Lee V, Whittankr L, Jaye C, Baroudi K M, Fischer D A and Banerjee S 2009 Chemistry of Materials 21 3905
[14]	Cote L J, Kim F and Huang J X 2009 J. Am. Chem. Soc. 131 1043
[15]	Kim F, Cote L J and Huang J X 2010 Adv. Mater. 22 1954
[16]	Li X L, Zhang G Y, Bai X D, Sun X M, Wang X R, Wang E G and Dai H J 2008 Nat. Nanotechnol. 3 538

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Preparation and characterization of PTFE coating in new polymer quartz piezoelectric crystal sensor for testing liquor products

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