High-pressure Raman study of MgV2O6 synthesized at high pressure and high temperature

doi:10.1088/1674-1056/22/6/066202

Abstract A new structural phase of MgV₂O₆ was obtained by a high-pressure, high-temperature (HPHT) synthesis method. The new phase was investigated by Rietveld analysis of X-ray powder diffraction data, showing space group Pbcn (No. 60) symmetry and a=13.6113(6) Å (1 Å=0.1 nm), b=5.5809(1) Å, c=4.8566(3) Å, V=368.93(2) Å³ (Z=4). High pressure behavior was studied by Raman spectroscopy at room temperature. Under 22.5 GPa, there was no sign of a structural phase transition in the spectra, demonstrating stability of the HPHT phase up to the highest pressure.

Keywords: high-pressure and high-temperature MgV₂O₆ Raman spectroscopy high-pressure

Received: 20 October 2012
Revised: 06 January 2013
Accepted manuscript online:

PACS:	62.50.-p	(High-pressure effects in solids and liquids)
	78.30.-j	(Infrared and Raman spectra)

Fund: Project supported by the National Natural Science Foundation of China (Grant No. 51172091) and the Program for New Century Excellent Talents in University.

Corresponding Authors: Wang Xin
E-mail: xin_wang@jlu.edu.cn

Cite this article:

Tang Rui-Lian (唐瑞莲), Li Yan (李岩), Tao Qiang (陶强), Li Na-Na (李娜娜), Li Hui (李会), Han Dan-Dan (韩丹丹), Zhu Pin-Wen (朱品文), Wang Xin (王欣) High-pressure Raman study of MgV₂O₆ synthesized at high pressure and high temperature 2013 Chin. Phys. B 22 066202

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High-pressure Raman study of MgV2O6 synthesized at high pressure and high temperature

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High-pressure Raman study of MgV₂O₆ synthesized at high pressure and high temperature