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Chin. Phys. B, 2008, Vol. 17(12): 4585-4591    DOI: 10.1088/1674-1056/17/12/042
CONDENSED MATTER: STRUCTURAL, MECHANICAL, AND THERMAL PROPERTIES Prev   Next  

Synthesis and photoluminescence property of boron carbide nanowires

Bao Li-Hong (鲍丽宏), Li Chen (李晨), Tian Yuan (田园), Tian Ji-Fa (田继发), Hui Chao (惠超), Wang Xing-Jun (王兴军), Shen Cheng-Min (申承民), Gao Hong-Jun (高鸿钧)
Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, Beijing 100190, China
Abstract  Large scale, high density boron carbide nanowires have been synthesized by using an improved carbothermal reduction method with B/B2O3/C powder precursors under an argon flow at 1100℃. The boron carbide nanowires are 5--10μm in length and 80--100nm in diameter. Transmission electron microscopy (TEM) and selected area electron diffraction (SAED) characterizations show that the boron carbide nanowire has a B4C rhombohedral structure with good crystallization. The Raman spectrum of the as-grown boron carbide nanowires is consistent with that of a B4C structure consisting of B11C icosahedra and C-B-C chains. The room temperature photoluminescence spectrum of the boron carbide nanowires exhibits a visible range of emission centred at 638nm.
Keywords:  carbothermal reduction      vapour-liquid-solid (VLS)      Raman      photoluminescence  
Received:  19 June 2008      Revised:  24 June 2008      Accepted manuscript online: 
PACS:  68.65.-k (Low-dimensional, mesoscopic, nanoscale and other related systems: structure and nonelectronic properties)  
  78.30.Hv (Other nonmetallic inorganics)  
  78.55.Hx (Other solid inorganic materials)  
  78.67.-n (Optical properties of low-dimensional, mesoscopic, and nanoscale materials and structures)  
  81.07.-b (Nanoscale materials and structures: fabrication and characterization)  
  81.16.-c (Methods of micro- and nanofabrication and processing)  
Fund: Project supported by the National High Technology Development Program of China (Grant No 2007AA03Z305) and the state Key Development Program for Basic Research of China (Grant No 2007CB935503) the National Science Foundation of China (Grants Nos 60571045,

Cite this article: 

Bao Li-Hong (鲍丽宏), Li Chen (李晨), Tian Yuan (田园), Tian Ji-Fa (田继发), Hui Chao (惠超), Wang Xing-Jun (王兴军), Shen Cheng-Min (申承民), Gao Hong-Jun (高鸿钧) Synthesis and photoluminescence property of boron carbide nanowires 2008 Chin. Phys. B 17 4585

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