Sputtering pressure influence on growth morphology, surface roughness, and electrical resistivity for strong anisotropy beryllium film
Luo Bing-Chi (罗炳池)a b, Li Kai (李恺)a b, Kang Xiao-Li (康晓丽)a, Zhang Ji-Qiang (张吉强)a, He Yu-Dan (何玉丹)a, Luo Jiang-Shan (罗江山)a, Wu Wei-Dong (吴卫东)a b, Tang Yong-Jian (唐永建)a
a Research Center of Laser Fusion, ChinaAcademy of Engineering Physics, Mianyang 621900, China; b Science and Technology on Plasma Physics Laboratory, Mianyang 621900, China
Abstract The strong anisotropy beryllium (Be) films are fabricated at different sputtering pressures by direct current magnetron sputtering. With the increase of pressure, the deposition rate of Be film first increases, and when the pressure exceeds 0.8 Pa, it gradually descends. The X-ray diffraction analysis indicates that Be film is of α-Be phase, its surface always reveals the (101) crystal plane possessing the low surface energy. As for the growth morphology of Be film, the surface is mainly characterized by the fibrous grains, while the cross section shows a transition from a columnar grain to a mixed grain consisting of a cone-shaped grain and a columnar grain as the sputtering pressure increases. The large grain fraction decays exponentially from 75.0% to 59.3% with the increase of sputtering pressure p, which can improve the grain size uniformity. The surface roughness increases due to the insufficient atom diffusion, which is comparable to its decrease due to the etching effect at p < 0.8 Pa, while it increases drastically at p > 0.8 Pa, and this increase is dominated by the atom diffusion. The electrical resistivity values of Be films range from 1.7 uΩ·m to 2.7 uΩ·m in the range 0.4 Pa-1.2 Pa, which is 50 times larger than the bulk resistivity.
Fund: Project supported by the National Natural Science Foundation of China (Grant No. 11204280).
Corresponding Authors:
Luo Jiang-Shan
E-mail: jiangshanluo@caep.ac.cn
Cite this article:
Luo Bing-Chi (罗炳池), Li Kai (李恺), Kang Xiao-Li (康晓丽), Zhang Ji-Qiang (张吉强), He Yu-Dan (何玉丹), Luo Jiang-Shan (罗江山), Wu Wei-Dong (吴卫东), Tang Yong-Jian (唐永建) Sputtering pressure influence on growth morphology, surface roughness, and electrical resistivity for strong anisotropy beryllium film 2014 Chin. Phys. B 23 066804
[1]
Haan S W, Herrmann M C and Amendt P A 2006 Fusion Sci. Technol. 49 553
[2]
Xu H W, Alford C S, Cooley J C, Dixon L A, Hackenberg R E, Letts S A, Moreno K A, Nikroo A, Wall J R and Youngblood K P 2007 Fusion Sci. Technol. 51 547
[3]
Haan S W, Amendt P A and Callahan D A 2007 Fusion Sci. Technol. 51 509
[4]
Moreno K A, Eddinger S and Fong J 2009 Fusion Sci. Technol. 55 349
[5]
Haan S W, Callahan D A and Edwards M J 2009 Fusion Sci. Technol. 55 227
[6]
Montgomery D S, Nobile A and Walsh P J 2004 Rev. Sci. Instrum. 75 3986
[7]
Davydov D A, Kholopova O V and Kolbasov B N 2007 J. Nucl. Mater. 367 1079
[8]
Nikroo A, Chen K C, Hoppe M L, Huang H, Wall J R, Xu H, McElfresh M W, Alford C S, Cook R C, Cooley J C, Fields R, Hackenberg R, Doerner R P and Baldwin M 2006 Phys. Plasmas 13 056302
[9]
Blum V, Rath Ch, Müller S, Hammer L and Heinz K 1999 Phys. Rev. B 59 15966
[10]
Singh S, Thiyagarajan P, Kant K M, Anita D, Thirupathiah S, Rama N, Tiwari B, Kottaisamy M and Rao M S R 2007 J. Phys. D: Appl. Phys. 40 6312
[11]
Chou C Y, Yao Y D, Kuo P C, Cheng K W and Yu C 2006 J. Magn. Magn. Mater. 304 e103
[12]
Yao X F, Wang J P, Zhou T J and Chong T C 2005 J. Appl. Phys. 93 8310
[13]
Tikhinskij G F, Stoev P I, Papirov I I, Babun V A and Vasilév A A 1996 J. Nucl. Mater. 233 828
[14]
Song D J, Zhang X M and Hu Q 2006 Mater. Rev. 20 66
[15]
Wang H P, Chang J and Wei B 2009 J. Appl. Phys. 106 033506
[16]
Ma X B, Wang H P, Zhou K, Chang J and Hong Z Y 2013 Appl. Phys. Lett. 103 104101
[17]
Zhu Z W, Gao X D, Zhang Z B, Piao Y H, Hu C, Zhang D W and Wu D P 2012 Chin. Phys. B 21 087304
[18]
Zhang L S, Yu H F and Guo Y Q 2012 Acta Phys. Sin. 61 016101 (in Chinese)
[19]
Lutišan J and Cvengroš J 1995 Chem. Eng. J. 56 39
[20]
Xie H B 1999 Vacuum 3 37
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