INTERDISCIPLINARY PHYSICS AND RELATED AREAS OF SCIENCE AND TECHNOLOGY |
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High thermal stability of diamond-cBN-B4C-Si composites |
Hong-Sheng Jia(贾洪声)1, Pin-Wen Zhu(朱品文)2, Hao Ye(叶灏)1, Bin Zuo(左斌)1, Yuan-Long E(鄂元龙)1, Shi-Chong Xu(徐仕翀)1, Ji Li(李季)1, Hai-Bo Li(李海波)1, Xiao-Peng Jia(贾晓鹏)2, Hong-An Ma(马红安)2 |
1. Key Laboratory of Functional Materials Physics and Chemistry of the Ministry of Education, Jilin Normal University, Siping 136000, China; 2. State Key Laboratory of Superhard Materials, Jilin University, Changchun 130012, China |
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Abstract Improving the thermal stability of diamond and other superhard materials has great significance in various applications. Here, we report the synthesis and characterization of bulk diamond-cBN-B4C-Si composites sintered at high pressure and high temperature (HPHT, 5.2 GPa, 1620-1680 K for 3-5 min). The results show that the diamond, cBN, B4C, BxSiC, SiO2 and amorphous carbon or a little surplus Si are present in the sintered samples. The onset oxidation temperature of 1673 K in the as-synthesized sample is much higher than that of diamond, cBN, and B4C. The high thermal stability is ascribed to the covalent bonds of B-C, C-N, and the solid-solution of BxSiC formed during the sintering process. The results obtained in this work may be useful in preparing superhard materials with high thermal stability.
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Received: 22 August 2016
Revised: 30 September 2016
Accepted manuscript online:
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PACS:
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81.05.uj
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(Diamond/nanocarbon composites)
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81.20.Ev
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(Powder processing: powder metallurgy, compaction, sintering, mechanical alloying, and granulation)
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81.70.Pg
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(Thermal analysis, differential thermal analysis (DTA), differential thermogravimetric analysis)
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Fund: Project supported by the National Natural Science Foundation of China (Grant No. 51301075) and the Project of Development and Reform Commission of Jilin Province, China (Grant No. 2014Y136). |
Corresponding Authors:
Pin-Wen Zhu, Hai-Bo Li
E-mail: zhupw@jlu.edu.cn;lihaibo@jlnu.edu.cn
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Cite this article:
Hong-Sheng Jia(贾洪声), Pin-Wen Zhu(朱品文), Hao Ye(叶灏), Bin Zuo(左斌), Yuan-Long E(鄂元龙), Shi-Chong Xu(徐仕翀), Ji Li(李季), Hai-Bo Li(李海波), Xiao-Peng Jia(贾晓鹏), Hong-An Ma(马红安) High thermal stability of diamond-cBN-B4C-Si composites 2017 Chin. Phys. B 26 018102
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