Please wait a minute...
Chin. Phys. B, 2022, Vol. 31(6): 060702    DOI: 10.1088/1674-1056/ac4902
GENERAL Prev   Next  

In-situ ultrasonic calibrations of pressure and temperature in a hinge-type double-stage cubic large volume press

Qingze Li(李青泽), Xiping Chen(陈喜平), Lei Xie(谢雷), Tiexin Han(韩铁鑫), Jiacheng Sun(孙嘉程), and Leiming Fang(房雷鸣)
Key Laboratory for Neutron Physics, Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang 621900, China
Abstract  Here, simultaneous in-situ calibration of pressures and temperatures was performed in a hinge-type second-stage cubic large volume press (LVP) up to 15 GPa and 1400 K by an acoustic travel-time approach. Based on the recently reported P-tS and P-T-tP-tS equations for Al2O3 buffer rod, the cell pressures and temperatures in the chamber of LVP were in-situ determined, in comparison with those by conventional off-line (or fixed-points) pressure calibration method and direct thermocouple measurement, respectively. It is found that the cell pressures of the LVP chamber are significantly reduced after annealing at simultaneous high pressures and high temperatures, owing to the stress relaxation as accumulate in the LVP chamber. This acoustic travel-time method is verified to be a good way for precise determination of thermal (cell) pressures at high temperature conditions, and is of great importance and necessity to conduct in-situ physical property measurements under extreme high P-T conditions, especially when the precious synchrotron x-ray/neutron diffraction beams are not available.
Keywords:  cubic press      simultaneous in-situ calibration of pressures and temperatures      acoustic travel-time      high pressure and high temperature  
Received:  02 November 2021      Revised:  27 December 2021      Accepted manuscript online:  07 January 2022
PACS:  07.35.+k (High-pressure apparatus; shock tubes; diamond anvil cells)  
  91.60.Gf (High-pressure behavior)  
  91.60.Lj (Acoustic properties)  
  43.35.Yb (Ultrasonic instrumentation and measurement techniques)  
Fund: Project supported by the National Natural Science Foundation of China (Grant Nos. 12075215, 11872198, and U2030110) and the National Key Research and Development Program of China (Grant No. 2016YFA0401503).
Corresponding Authors:  Leiming Fang     E-mail:

Cite this article: 

Qingze Li(李青泽), Xiping Chen(陈喜平), Lei Xie(谢雷), Tiexin Han(韩铁鑫), Jiacheng Sun(孙嘉程), and Leiming Fang(房雷鸣) In-situ ultrasonic calibrations of pressure and temperature in a hinge-type double-stage cubic large volume press 2022 Chin. Phys. B 31 060702

[1] Sokol A G, Borzdov Y M, Palyanov Y N and Khokhryakov A F 2015 High Pressure Res. 35 139
[2] Frost D J, Poe B T, Nnes R G, Liebske C, Duba A and Rubie D C 2004 Phys. Earth Planet. Inter. 143 507
[3] Takayuki I, Liu Z D and Katsura T 2019 Engineering 5 434
[4] Xie L, Yoneda A, Yoshino T, Yamazaki D, Tsujino N, Higo Y and Ito E 2017 Rev. Sci. Instrum. 88 093904
[5] Fang L M, He D W, Chen C, Ding L Y and Luo X J 2007 High Pressure Res. 27 367
[6] Katsura T, Yamada H, Nishikawa O, Song M, Kubo A, Shinmei T and Funakoshi K I 2004 J. Geophys. Res. 109 B02209
[7] Higo Y, Irifune T and Funakoshi K 2018 Rev. Sci. Instrum. 89 014501
[8] Zhang J W, He D W, Fang L M, Hu Q W, Li X, Li Q, Wang J P and Wang Y P 2020 Rev. Sci. Instrum. 91 125103
[9] Shang Y C, Shen F R, Hou X Y, Chen L Y, Hu K, Li X, Liu R, Tao Q, Zhu P W, Liu Z D, Yao M G, Zhou Q, Cui T and Liu B B 2020 Chin. Phys. Lett. 37 080701
[10] Decker D L 1971 J. Appl. Phys. 42 3239
[11] Anderson O L, Isaak D G and Yamamoto S 1989 J. Appl. Phys. 65 1534
[12] Dorfman S M, Prakapenka V B, Meng Y and Duffy T S 2012 J. Geophys. Res. 117 B08210
[13] Dorogokupets P I and Oganov A R 2007 Phys. Rev. B 75 024115
[14] Bean V E, Akimoto S, Bell P M, Block S, Holzapfel W B, Manghnani M H, Nicol M F and Stishov S M 1986 Physica B+C 139 52
[15] Xu C, He D W, Wang H K, Wang W D, Tang M J and Wang P 2014 Chin. Sci. Bull. 59 5251
[16] Decker D, Bassett W A, Merrill L, Hall H T and Barnett J D 1972 J. Phys. Chem. Ref. Data 1 773
[17] Fei Y, Ricolleau A, Frank M, Mibe K, Shen G and Prakapenka V B 2007 Proc. Natl. Acad. Sci. USA 104 9182
[18] Bohlen S R and Boettcher A L 1982 J. Geophys. Res. 87(B8) 7073
[19] Wang X B, Chen T, Qi X T, Zou Y T, Kung J, Yu T, Wang Y B, Liebermann R C and Li B S 2015 J. Appl. Phys. 118 065901
[20] Higo Y, Inoue T, Li B S, Irifune T and Liebermann R C 2006 Phys. Earth Planet. Inter. 159 276
[21] Song W, Shan S M, Tang Q Z, Su C and Liu Y G 2021 Acta Geochim. 40 525
[22] Fang L M, Chen X P, Xie L, He D W, Hu Q W, Li X, Jiang M Q, Sun G A, Chen B, Peng S M, Li H and Han T X 2020 Chin. J. High Pressure Phys. 34 050104
[23] Xu C W, Li Y, Inoue T, Gréaux S, Li Q Z, Gao J, Sun F X and Fang L M 2021 High Pressure Res. 41 233
[24] Li Q Z, Yang X X, Peng F, Yang G Z, Han T X, Fang L M, Hu Q W, Xie L, Chen X P and Zou Y T 2021 J. Eur. Ceramic Soc. 41 4788
[25] Wu B B, Lei L, Zhang F, Tang Q Q, Liu S, Pu M F, He D W, Xia Y H, Fang L M, Ohfuji H and Irifune T 2021 Matter Radiat. Extreme 6 038401
[26] Liang H, Fang L M, Guan S X, Peng F, Zhang Z G, Chen H H, Zhang W and Lu C 2021 Inorg. Chem. 60 515
[27] Li B S, Jackson I, Gasparik T and Liebermann R C 1996 Phys. Earth Planet. Inter. 98 79
[28] Li B S, Kung J, Liu W and Liebermann R C 2014 Phys. Earth Planet. Inter. 228 63
[29] Cai N, Chen T, Qi X T and Li B S 2018 J. Appl. Phys. 124 185901
[30] Gieske J H and Barsch G R 1968 Phys. Status Solidi 29 121
[31] Nishiharav Y, Doi S, Kakizawa S, Higo Y and Tange Y 2019 Phys. Earth Planet. Inter. 298 106348
[1] Synergistic influences of titanium, boron, and oxygen on large-size single-crystal diamond growth at high pressure and high temperature
Guang-Tong Zhou(周广通), Yu-Hu Mu(穆玉虎), Yuan-Wen Song(宋元文), Zhuang-Fei Zhang(张壮飞), Yue-Wen Zhang(张跃文), Wei-Xia Shen(沈维霞), Qian-Qian Wang(王倩倩), Biao Wan(万彪), Chao Fang(房超), Liang-Chao Chen(陈良超), Ya-Dong Li(李亚东), and Xiao-Peng Jia(贾晓鹏). Chin. Phys. B, 2022, 31(6): 068103.
[2] Dependence of nitrogen vacancy color centers on nitrogen concentration in synthetic diamond
Yong Li(李勇), Xiaozhou Chen(陈孝洲), Maowu Ran(冉茂武), Yanchao She(佘彦超), Zhengguo Xiao(肖政国), Meihua Hu(胡美华), Ying Wang(王应), and Jun An(安军). Chin. Phys. B, 2022, 31(4): 046107.
[3] Synthesis and characterizations of boron and nitrogen co-doped high pressure and high temperature large single-crystal diamonds with increased mobility
Xin-Yuan Miao(苗辛原), Hong-An Ma(马红安), Zhuang-Fei Zhang(张壮飞), Liang-Chao Chen(陈良超), Li-Juan Zhou(周丽娟), Min-Si Li(李敏斯), and Xiao-Peng Jia(贾晓鹏). Chin. Phys. B, 2021, 30(6): 068102.
[4] Utilizing of high-pressure high-temperature synthesis to enhance the thermoelectric properties of Zn0.98Al0.02O with excellent electrical properties
Qi Chen(陈启), Xinjian Li(李欣健), Yao Wang(王遥), Lijie Chang(常立杰), Jian Wang(王健), Yuewen Zhang(张跃文), Hongan Ma(马红安), and Xiaopeng Jia(贾晓鹏). Chin. Phys. B, 2021, 30(1): 016202.
[5] A double-layer heating method to generate high temperature in a two-stage multi-anvil apparatus
Bo Peng(彭博), Zili Kou(寇自力), Mengxi Zhao(赵梦溪), Mingli Jiang(姜明莉), Jiawei Zhang(张佳威), Yipeng Wang(王义鹏), Lu Zhang(张陆). Chin. Phys. B, 2020, 29(9): 090703.
[6] Crystallization and characteristics of {100}-oriented diamond with CH4N2S additive under high pressure and high temperature
Yong Li(李勇), Debing Tan(谭德斌), Qiang Wang(王强), Zhengguo Xiao(肖政国), Changhai Tian(田昌海), Lin Chen(陈琳). Chin. Phys. B, 2020, 29(9): 098103.
[7] Congruent melting of tungsten phosphide at 5 GPa and 3200℃ for growing its large single crystals
Xiao-Jun Xiang(向晓君), Guo-Zhu Song(宋国柱), Xue-Feng Zhou(周雪峰), Hao Liang(梁浩), Yue Xu(徐月), Shi-Jun Qin(覃湜俊), Jun-Pu Wang(王俊普), Fang Hong(洪芳), Jian-Hong Dai(戴建红), Bo-Wen Zhou(周博文), Wen-Jia Liang(梁文嘉), Yun-Yu Yin(殷云宇), Yu-Sheng Zhao(赵予生), Fang Peng(彭放), Xiao-Hui Yu(于晓辉), Shan-Min Wang(王善民). Chin. Phys. B, 2020, 29(8): 088202.
[8] Regulation mechanism of catalyst structure on diamond crystal morphology under HPHT process
Ya-Dong Li(李亚东), Yong-Shan Cheng(程永珊), Meng-Jie Su(宿梦洁), Qi-Fu Ran(冉启甫), Chun-Xiao Wang(王春晓), Hong-An Ma(马红安), Chao Fang(房超), Liang-Chao Chen(陈良超). Chin. Phys. B, 2020, 29(7): 078101.
[9] High pressure and high temperature induced polymerization of C60 quantum dots
Shi-Hao Ruan(阮世豪), Chun-Miao Han(韩春淼), Fu-Lu Li(李福禄), Bing Li(李冰), Bing-Bing Liu(刘冰冰). Chin. Phys. B, 2020, 29(2): 026402.
[10] Synthesis of black phosphorus structured polymeric nitrogen
Ying Liu(刘影)†, Haipeng Su(苏海鹏), Caoping Niu(牛草萍), Xianlong Wang(王贤龙), Junran Zhang(张俊然), Zhongxue Ge(葛忠学), and Yanchun Li(李延春). Chin. Phys. B, 2020, 29(10): 106201.
[11] Characteristics of urea under high pressure and high temperature
Shuai Fang(房帅), Hong-An Ma(马红安), Long-Suo Guo(郭龙锁), Liang-Chao Chen(陈良超), Yao Wang(王遥), Lu-Yao Ding(丁路遥), Zheng-Hao Cai(蔡正浩), Jian Wang(王健), Xiao-Peng Jia(贾晓鹏). Chin. Phys. B, 2019, 28(9): 098101.
[12] Inclusions in large diamond single crystals at different temperatures of synthesis
Fei Han(韩飞), Shang-Sheng Li(李尚升), Xue-Fei Jia(贾雪菲), Wei-Qin Chen(陈玮琴), Tai-Chao Su(宿太超), Mei-Hua Hu(胡美华), Kun-Peng Yu(于昆鹏), Jian-Kang Wang(王健康), Yu-Min Wu(吴玉敏), Hong-An Ma(马红安), Xiao-Peng Jia(贾晓鹏). Chin. Phys. B, 2019, 28(2): 028103.
[13] Synthesis of diamonds in Fe—C systems using nitrogen and hydrogen co-doped impurities under HPHT
Shi-Shuai Sun(孙士帅), Zhi-Hui Xu(徐智慧), Wen Cui(崔雯), Xiao-Peng Jia(贾晓鹏), Hong-An Ma(马红安). Chin. Phys. B, 2017, 26(9): 098101.
[14] Different effect of NiMnCo or FeNiCo on the growth of type-IIa large diamonds with Ti/Cu as nitrogen getter
Shang-Sheng Li(李尚升), He Zhang(张贺), Tai-Chao Su(宿太超), Qiang Hu(胡强), Mei-Hua Hu(胡美华), Chun-Sheng Gong(龚春生), Hon-An Ma(马红安), Xiao-Peng Jia(贾晓鹏), Yong Li(李勇). Chin. Phys. B, 2017, 26(6): 068102.
[15] Synthesis of N-type semiconductor diamonds with sulfur, boron co-doping in FeNiMnCo-C system at high pressure and high temperature
He Zhang(张贺), Shangsheng Li(李尚升), Taichao Su(宿太超), Meihua Hu(胡美华), Hongan Ma(马红安), Xiaopeng Jia(贾晓鹏), Yong Li(李勇). Chin. Phys. B, 2017, 26(5): 058102.
No Suggested Reading articles found!