In-situ SAXS study on PET/ PMMT composites during tensile tests

doi:10.1088/1674-1056/25/1/017802

Abstract The nanostructures during the tensile drawing of poly(ethylene terephthalate) (PET)/hexadecyl triphenyl phosphonium bromide montmorillonite (PMMT) nanocomposites were studied by in-situ small angle x-ray scattering. For strain higher than the yield point, the scattering intensity increases dramatically due to the nucleation and growth of nanovoids and crystals. The nanovoids and crystals are significantly dependent on the heating temperature. The effective filling of PMMT in the PET matrix provokes a strong restriction to the long period. The peaks of the long period disappear gradually with the deformation strain increasing from 0% to 34%.

Keywords: small angle x-ray scattering nanostructure montmorillonite poly(ethylene terephthalate)

Received: 16 July 2015
Revised: 24 September 2015
Accepted manuscript online:

PACS:

78.70.Ck

(X-ray scattering)

Fund: Project supported by the National Natural Science Foundation of China (Grant Nos. U1232203, U1432104, U1332107, 11305198, and 11405199), the Program for Young Teachers Scientific Research in Qiqihar University, China (Grant No. 2012k-Z02), and the Natural Science Foundation of Heilongjiang Province, China (Grant No. E201259).

Corresponding Authors: Wei-Dong Cheng, Xiao-Hua Gu
E-mail: 57399942@qq.com;gxh216@163.com

Cite this article:

Wei-Dong Cheng(程伟东), Xiao-Hua Gu(顾晓华), Xue Song(宋雪), Peng Zeng(曾鹏), Zhao-Jun Wu(吴昭君), Xue-Qing Xing(邢雪青), Guang Mo(默广), Zhong-Hua Wu(吴忠华) In-situ SAXS study on PET/ PMMT composites during tensile tests 2016 Chin. Phys. B 25 017802

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In-situ SAXS study on PET/ PMMT composites during tensile tests

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