A DOUBLE-TEMPERATURE-GRADIENT TECHNIQUE FOR THE GROWTH OF PURE C60 SINGLE CRYSTALS FROM THE VAPOR PHASE

doi:10.1088/1004-423X/3/5/006

Abstract

Abstract Pure C₆₀ single crystals were grown by a sublimation-condensation method in an evacuated dosed quartz tube situated in a double-temperature-gradient furnace. Large C₆₀ single crystals, up to a size of 0.6 mm×1.0 mm×2.0 mm with quite smooth and shiny faces, were obtained. X-ray diffraction, electron diffraction and X-ray morphology were carried out and showed that the quality of large C₆₀ single crystals grown by the double-temperature-gradient technique is excellent. In this paper the experimental results of the growth of large C₆₀ single crystals are reported and the morphological and structural characterizations are discussed in detail.

Received: 04 October 1993
Accepted manuscript online:

PACS:	81.10.Bk	(Growth from vapor)
	61.48.-c	(Structure of fullerenes and related hollow and planar molecular structures)
	61.05.cp	(X-ray diffraction)
	61.05.J-	(Electron diffraction and scattering)

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WANG GANG (王刚), XIE SI-SHEN (解思深), LIU WEI (刘维), FU CHUN-SHENG (傅春生), LI CHAO-RONG (李超荣), WANG CHANG-QING (王昌庆), LI NAN (李楠), QIAN SHENG-FA (钱生法), ZHANG ZE-BO (张泽勃), YU YU-DE (俞育德), ZHOU WEI-YA (周维亚) A DOUBLE-TEMPERATURE-GRADIENT TECHNIQUE FOR THE GROWTH OF PURE C₆₀ SINGLE CRYSTALS FROM THE VAPOR PHASE 1994 Acta Physica Sinica (Overseas Edition) 3 360

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A DOUBLE-TEMPERATURE-GRADIENT TECHNIQUE FOR THE GROWTH OF PURE C60 SINGLE CRYSTALS FROM THE VAPOR PHASE

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A DOUBLE-TEMPERATURE-GRADIENT TECHNIQUE FOR THE GROWTH OF PURE C₆₀ SINGLE CRYSTALS FROM THE VAPOR PHASE