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Chemical synthesis of zinc oxide nanorods for enhanced hydrogen gas sensing |
Musarrat Jabeena, Muhammad Azhar Iqbala, R Vasant Kumarb, Mansoor Ahmeda, Muhammad Tayyeb Javedc |
a Department of Physics, University of the Punjab Lahore, Pakistan; b Department of Material Science and Metallurgy, University of Cambridge, England; c Department of Chemical Engineering, Pakistan Institute of Engineering and Applied Sciences, Nilore, Islamabad, Pakistan |
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Abstract Zinc oxide (ZnO) nanorods are prepared using equimolar solution of zinc nitrate ((Zn(NO3)2) and hexamethylenetetramine (C6H12N4) by the hydrothermal technique at 80 ℃ for 12 h. Epitaxial growth is explored by X-ray diffraction (XRD) patterns, revealing that the ZnO nanorods have a hexagonal (wurtzite) structure. Absorption spectra of ZnO are measured by UV–visible spectrometer. The surface morphology is investigated by field emission scanning electron microscopy (FESEM). The synthesized ZnO nanorods are used for detecting the 150 ℃ hydrogen gas with a concentration over 1000 ppm. The obtained results show a reversible response. The influence of operating temperature on hydrogen gas detecting characteristic of ZnO nanorods is also investigated.
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Received: 25 April 2013
Revised: 02 July 2013
Accepted manuscript online:
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PACS:
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85.85.+j
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(Micro- and nano-electromechanical systems (MEMS/NEMS) and devices)
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85.35.-p
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(Nanoelectronic devices)
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81.07.-b
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(Nanoscale materials and structures: fabrication and characterization)
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Fund: Projected supported by the HEC of Pakistan for international initiative research support programme (IRSIP). |
Corresponding Authors:
Musarrat Jabeen
E-mail: musarrat95@hotmail.com
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Cite this article:
Musarrat Jabeen, Muhammad Azhar Iqbal, R Vasant Kumar, Mansoor Ahmed, Muhammad Tayyeb Javed Chemical synthesis of zinc oxide nanorods for enhanced hydrogen gas sensing 2014 Chin. Phys. B 23 018504
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