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Pre-existing orthorhombic embryos-induced hexagonal—orthorhombic martensitic transformation in MnNiSi1-x(CoNiGe)x alloy |
| Ting-Ting Zhang(张婷婷), Yuan-Yuan Gong(龚元元), Zi-Qian Lu(鲁子骞), and Feng Xu(徐锋)† |
| MIIT Key Laboratory of Advanced Metallic and Intermetallic Materials Technology, School of Materials Science and Engineering, Nanjing University of Science and Technology, Nanjing 210094, China |
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Abstract The thermal—elastic martensitic transformation from high-temperature Ni$_{2}$In-type hexagonal structure to low-temperature TiNiSi-type orthorhombic structure has been widely studied in Mn$MX$ ($M={\rm Ni}$ or Co, and $X={\rm Ge}$ or Si) alloys. However, the answer to how the orthorhombic martensite nucleates and grows within the hexagonal parent is still unclear. In this work, the hexagonal—orthorhombic martensitic transformation in a Co and Ge co-substituted MnNiSi is investigated. One can find some orthorhombic laths embedded in the hexagonal parent at a temperature above the martensitic transformation start temperature ($M_{\rm s}$). With the the sample cooing to $M_{\rm s}$, the laths turn broader, indicating that the martensitic transformation starts from these pre-existing orthorhombic laths. Microstructure observation suggests that these pre-existing orthorhombic laths do not originate from the hexagonal—orthorhombic martensitic transformation because of the difference between atomic occupations of doping elements in the hexagonal parent and those in the pre-existing orthorhombic laths. The phenomenological crystallographic theory and experimental investigations prove that the pre-existing orthorhombic lath and generated orthorhombic martensite have the same crystallography relationship to the hexagonal parent. Therefore, the orthorhombic martensite can take these pre-existing laths as embryos and grow up. This work implies that the martensitic transformation in MnNiSi$_{1-x}$(CoNiGe)$_{x}$ alloy is initiated by orthorhombic embryos.
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Received: 18 September 2023
Revised: 17 December 2023
Accepted manuscript online: 25 December 2023
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PACS:
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81.30.Kf
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(Martensitic transformations)
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81.05.Bx
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(Metals, semimetals, and alloys)
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68.55.A-
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(Nucleation and growth)
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61.50.Ks
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(Crystallographic aspects of phase transformations; pressure effects)
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| Fund: Project supported by the National Natural Science Foundation of China (Grant No. 11974184). |
Corresponding Authors:
Feng Xu
E-mail: xufeng@njust.edu.cn
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Cite this article:
Ting-Ting Zhang(张婷婷), Yuan-Yuan Gong(龚元元), Zi-Qian Lu(鲁子骞), and Feng Xu(徐锋) Pre-existing orthorhombic embryos-induced hexagonal—orthorhombic martensitic transformation in MnNiSi1-x(CoNiGe)x alloy 2024 Chin. Phys. B 33 048103
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