Gas encapsulation technology for large volume press

doi:10.1088/1674-1056/ad7af8

中国物理B ›› 2024, Vol. 33 ›› Issue (11): 110701-110701.doi: 10.1088/1674-1056/ad7af8

Gas encapsulation technology for large volume press

Minghao Du(杜明浩) and Duanwei He(贺端威)†

Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065, China

收稿日期:2024-05-13 修回日期:2024-07-31 接受日期:2024-09-14 出版日期:2024-11-15 发布日期:2024-11-15
基金资助:
This study was supported by the National Key R&D Program of China (Grant No. 2023YFA1406200).

Gas encapsulation technology for large volume press

Minghao Du(杜明浩) and Duanwei He(贺端威)†

Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065, China

Received:2024-05-13 Revised:2024-07-31 Accepted:2024-09-14 Online:2024-11-15 Published:2024-11-15
Contact: Duanwei He E-mail:duanweihe@scu.edu.cn
Supported by:
This study was supported by the National Key R&D Program of China (Grant No. 2023YFA1406200).

摘要/Abstract

摘要： For samples in the gaseous state at room temperature and ambient pressure, mature technology has been developed to encapsulate them in a diamond anvil cell (DAC). However, the large volume press (LVP) can only treat samples with starting materials in solid or liquid form. We have achieved stable encapsulation and reaction treatment of carbon dioxide in a centimeter sized sample chamber for a long time (over 10 min) under conditions of temperature higher than 1200 ℃ and pressure over 5 GPa through the use of integrated low-temperature freezing and rapid compression sealing method for LVP cell assemblies. This technology can also be applied to the packaging of other gaseous or liquid samples, such as ammonia, sulfur dioxide, water, etc. in LVP devices.

关键词: large volume press, gas encapsulation, low-temperature

Abstract: For samples in the gaseous state at room temperature and ambient pressure, mature technology has been developed to encapsulate them in a diamond anvil cell (DAC). However, the large volume press (LVP) can only treat samples with starting materials in solid or liquid form. We have achieved stable encapsulation and reaction treatment of carbon dioxide in a centimeter sized sample chamber for a long time (over 10 min) under conditions of temperature higher than 1200 ℃ and pressure over 5 GPa through the use of integrated low-temperature freezing and rapid compression sealing method for LVP cell assemblies. This technology can also be applied to the packaging of other gaseous or liquid samples, such as ammonia, sulfur dioxide, water, etc. in LVP devices.

Key words: large volume press, gas encapsulation, low-temperature

中图分类号: (High-pressure apparatus; shock tubes; diamond anvil cells)

07.35.+k

82.40.Fp (Shock wave initiated reactions, high-pressure chemistry)

Minghao Du(杜明浩) and Duanwei He(贺端威). Gas encapsulation technology for large volume press[J]. 中国物理B, 2024, 33(11): 110701-110701.

Minghao Du(杜明浩) and Duanwei He(贺端威). Gas encapsulation technology for large volume press[J]. Chin. Phys. B, 2024, 33(11): 110701-110701.

参考文献

[1] Tian Y, Xu B, Yu D, et al. 2013 Nature 493 385
[2] Xu C, He D, Wang H, et al. 2013 S. Int. J. Refract. Met. H 36 232
[3] Guan S, Fang P, Hao L, et al. 2018 J. Appl. Phys. 124 215902
[4] Tetsuo I, Kurio A, Sakamoto S, et al. 2004 Phys. Earth. Planet. In. 143 593600
[5] Qin J, He D, Wang J, et al. 2008 AEnM 20 4780
[6] Wang S, Antonio D, Yu X, et al. 2015 Sci. Rep. 5 9
[7] Zhang J, He D, Fang L, et al. 2020 Rev. Sci. Instrum. 91 125103
[8] Liu G, Kou Z, Yan X, et al. 2015 Appl. Phys. Lett. 106 121901
[9] Druzhbin D and Myhill R 2016 Rev. Sci. Instrum. 87 024501
[10] Shang Y, Shen F, Hou X, et al. 2020 Chin. Phys. Lett. 37 80701
[11] Xi L, Chen J, Tang J, et al. 2012 High. Pressure. Res. 32 239
[12] Daniil K, Serovaiskii A, et al. 2017 J. Phys. Chem. A 121 6004
[13] Jayasooriya U A and Kettle S F A 1952 J. Phys. Chem. A 89 94447
[14] Alexander K, Innokenty K, Boffa-Ballaran, et al. 2008 Rev. Sci. Instrum. 4 045110
[15] Takemura K, Sahu P C, Yoshiyasu, et al. 2001 Rev. Sci. Instrum. 72 387376
[16] Bernard C, Noël D, Hamel, et al. 2003 High. Pressure. Res. 23 40915
[17] Shin-ichi M, Hisako H, Hirotada G, et al. 2010 Rev. Sci. Instrum. 81 033901
[18] Klotz S, Chervin J C, Munsch P, et al. 2009 Appl. Phys. 42 075413
[19] Dewaele A and Loubeyre P 2007 High. Pressure. Res. 27 41929
[20] Varga T, Wilkinson A P and Angel R J 2003 Rev. Sci. Instrum. 74 456466
[21] Hikita T, Maruyama T and Yamada N 1990 Jpn. J. Appl. Phys. 29 251925
[22] Zhang J, Liu F, Wu J, et al. 2018 Rev. Sci. Instrum. 89 075106
[23] Zhang J, He D, Fang L, et al. 2020 Rev. Sci. Instrum. 91 125103
[24] Huang M, Peng F, Guan S, et al. 2021 Rev. Sci. Instrum. 92 073903
[25] Yan X, Ren X, He D, et al. 2016 Rev. Sci. Instrum. 87 125006
[26] Zeto R J and Vanfleet H B 1969 J. Appl. Phys. 40 222731
[27] Jing Q, Yan B, Qiang W, et al. 2007 Rev. Sci. Instrum. 78 073906
[28] Giordano Valentina M, Frédéric D and Agnès D 2006 J. Chem. Phys. 8 125

Gas encapsulation technology for large volume press

Gas encapsulation technology for large volume press

PDF (PC)

赞

可视化

摘要/Abstract

引用本文

使用本文

参考文献

相关文章 15

Metrics

本文评价

推荐阅读 0

[1]	Xiang Guan(关翔), Jie Fan(樊洁), Yong-Bo Bian(边勇波), Zhi-Gang Cheng(程智刚), and Zhong-Qing Ji(姬忠庆). Development of 400-μW cryogen-free dilution refrigerators for quantum experiments[J]. 中国物理B, 2024, 33(7): 70701-070701.
[2]	Si-Si Tu(涂思思), Lei Liu(刘雷), Bo Zhou(周波), Chuang-Hui Dong(董创辉), Li-Ming Ye(叶力铭), Ying-Li Sun(孙颖莉), Yong Ding(丁勇), A-Ru Yan(闫阿儒), and Xin-Biao Mao(毛信表). Effect of spin-reorientation transition of cell boundary phases on the temperature dependence of magnetization and coercivity in Sm₂Co₁₇ magnets[J]. 中国物理B, 2023, 32(12): 127501-127501.
[3]	Xin Liu(刘欣), Qing-Hao Meng(孟庆昊), Jing Ding(丁晶), Zhi-Chen Bai(白志晨), Jia-Hui Wang(王佳慧), Cong Zhang(张聪), Bo Su(苏波), and Cun-Lin Zhang(张存林). Terahertz generation and detection of LT-GaAs thin film photoconductive antennas excited by lasers of different wavelengths[J]. 中国物理B, 2022, 31(2): 28701-028701.
[4]	Yang-Yan Guo(郭仰岩), Wei-Hua Han(韩伟华), Xiao-Di Zhang(张晓迪), Jun-Dong Chen(陈俊东), and Fu-Hua Yang(杨富华). Observation of source/drain bias-controlled quantum transport spectrum in junctionless silicon nanowire transistor[J]. 中国物理B, 2022, 31(1): 17701-017701.
[5]	刘东, 曲国峰, 王占辉, 王华杰, 刘灏, 王艺舟, 徐子虚, 李敏, 杨朝文, 刘星泉, 林炜平, 颜敏, 黄宇, 朱宇轩, 许敏, 韩纪锋. Interaction of supersonic molecular beam with low-temperature plasma[J]. 中国物理B, 2020, 29(6): 65208-065208.
[6]	郭辉, 陈辉, 阙炎德, 郑琦, 张余洋, 鲍丽宏, 黄立, 王业亮, 杜世萱, 高鸿钧. Low-temperature growth of large-scale, single-crystalline graphene on Ir(111)[J]. 中国物理B, 2019, 28(5): 56107-056107.
[7]	陈书真, 宋力刚, 张鹏, 曹兴忠, 于润升, 王宝义, 魏龙, 张仁刚. Influence of low-temperature sulfidation on the structure of ZnS thin films[J]. 中国物理B, 2019, 28(2): 24214-024214.
[8]	徐玉青, 汪尧进, 王一平, 杨颖, 袁国亮. CuO added Pb_0.92Sr_0.06Ba_0.02(Mg_1/3Nb_2/3)_0.25(Ti_0.53Zr_0.47)_0.75O₃ ceramics sintered with Ag electrodes at 900℃ for multilayer piezoelectric actuator[J]. 中国物理B, 2017, 26(3): 37702-037702.
[9]	王磊, 张家琦, 李柳暗, 前田裕太郎, 敖金平. Plasma-assisted surface treatment for low-temperature annealed ohmic contact on AlGaN/GaN heterostructure field-effect transistors[J]. 中国物理B, 2017, 26(3): 37201-037201.
[10]	郭新格, 林建超, 童鹏, 蔺帅, 杨骋, 鲁文建, 宋文海, 孙玉平. Anomalous low-temperature heat capacity in antiperovskite compounds[J]. 中国物理B, 2017, 26(2): 26501-026501.
[11]	徐宁, 李建福, 黄勃龙, 王保林. A new family of sp³-hybridized carbon phases[J]. 中国物理B, 2016, 25(1): 16103-016103.
[12]	徐宁, 李建福, 黄勃龙, 王保林. Low-temperature phase transformation from nanotube to sp³ superhard carbon phase[J]. 中国物理B, 2015, 24(6): 66102-066102.
[13]	杜丽军, 宋红芳, 李海霞, 陈邵龙, 陈婷, 孙焕尧, 黄垚, 童昕, 管桦, 高克林. Determination of ion quantity by using low-temperature ion density theory and molecular dynamics simulation[J]. 中国物理B, 2015, 24(11): 113703-113703.
[14]	窦刚, 李玉霞, 郭梅. Dual-band LTCC antenna based on 0.95Zn₂SiO₄-0.05CaTiO₃ ceramics for GPS/UMTS applications[J]. 中国物理B, 2015, 24(10): 108401-108401.
[15]	贾瑞龙, 苏桦, 唐晓莉, 荆玉兰. Effects of BaCu(B₂O₅) addition on sintering temperature and microwave dielectric properties of Ba₅Nb₄O₁₅-BaWO₄ ceramics[J]. 中国物理B, 2014, 23(4): 47801-047801.