Synthesis, structure, and properties of Ba9Co3Se15 with one-dimensional spin chains

doi:10.1088/1674-1056/ab69ea

中国物理B ›› 2020, Vol. 29 ›› Issue (3): 36102-036102.doi: 10.1088/1674-1056/ab69ea

• CONDENSED MATTER: STRUCTURAL, MECHANICAL, AND THERMAL PROPERTIES • 上一篇下一篇

Synthesis, structure, and properties of Ba₉Co₃Se₁₅ with one-dimensional spin chains

Lei Duan(段磊), Xian-Cheng Wang(望贤成), Jun Zhang(张俊), Jian-Fa Zhao(赵建发), Li-Peng Cao(曹立朋), Wen-Min Li(李文敏), Run-Ze Yu(于润泽), Zheng Deng(邓正), Chang-Qing Jin(靳常青)

1 Institute of Physics, Chinese Academy of Sciences, Beijing 100190, China;
2 School of Physics, University of Chinese Academy of Sciences, Beijing 100190, China;
3 Materials Research Laboratory at Songshan Lake, Dongguan 523808, China

收稿日期:2019-11-26 修回日期:2020-01-06 出版日期:2020-03-05 发布日期:2020-03-05
通讯作者: Xian-Cheng Wang, Chang-Qing Jin E-mail:wangxiancheng@aphy.iphy.ac.cn;jin@iphy.ac.cn
基金资助:
Project supported by the National Key R&D Program of China and the National Natural Science Foundation of China (Grant Nos. 2018YFA0305700, 2017YFA0302900, 11974410, and 11534016).

Synthesis, structure, and properties of Ba₉Co₃Se₁₅ with one-dimensional spin chains

Lei Duan(段磊)^1,2, Xian-Cheng Wang(望贤成)¹, Jun Zhang(张俊)^1,2, Jian-Fa Zhao(赵建发)^1,2, Li-Peng Cao(曹立朋)^1,2, Wen-Min Li(李文敏)^1,2, Run-Ze Yu(于润泽)¹, Zheng Deng(邓正)¹, Chang-Qing Jin(靳常青)^1,2,3

1 Institute of Physics, Chinese Academy of Sciences, Beijing 100190, China;
2 School of Physics, University of Chinese Academy of Sciences, Beijing 100190, China;
3 Materials Research Laboratory at Songshan Lake, Dongguan 523808, China

Received:2019-11-26 Revised:2020-01-06 Online:2020-03-05 Published:2020-03-05
Contact: Xian-Cheng Wang, Chang-Qing Jin E-mail:wangxiancheng@aphy.iphy.ac.cn;jin@iphy.ac.cn
Supported by:
Project supported by the National Key R&D Program of China and the National Natural Science Foundation of China (Grant Nos. 2018YFA0305700, 2017YFA0302900, 11974410, and 11534016).

摘要/Abstract

摘要： A new compound with one-dimensional spin chains, Ba₉Co₃Se₁₅, was synthesized under high pressure and high temperature conditions and systematically characterized via structural, transport and magnetic measurements. Ba₉Co₃Se₁₅ crystallizes in a hexagonal structure with the space group P-6c2 (No. 188) and lattice constants of a =b = 9.6765 Å and c = 18.9562 Å. The structure consists of trimeric face-sharing octahedral CoSe₆ chains, which are arranged in a triangular lattice in the ab-plane and separated by Ba atoms. The distance of the nearest neighbor of CoSe₆ chains is very large, given by the lattice constant a= 9.6765 Å. The Weiss temperature T_θ associated with the intra-chain coupling strength is about -346 K. However, no long-range magnetic order but a spin glass transition at ~3 K has been observed. Our results indicate that the spin glass behavior in Ba₉Co₃Se₁₅ mainly arises from the magnetic frustration due to the geometrically frustrated triangular lattice.

关键词: one-dimensional chain, spin glass, high-pressure

Abstract: A new compound with one-dimensional spin chains, Ba₉Co₃Se₁₅, was synthesized under high pressure and high temperature conditions and systematically characterized via structural, transport and magnetic measurements. Ba₉Co₃Se₁₅ crystallizes in a hexagonal structure with the space group P-6c2 (No. 188) and lattice constants of a =b = 9.6765 Å and c = 18.9562 Å. The structure consists of trimeric face-sharing octahedral CoSe₆ chains, which are arranged in a triangular lattice in the ab-plane and separated by Ba atoms. The distance of the nearest neighbor of CoSe₆ chains is very large, given by the lattice constant a= 9.6765 Å. The Weiss temperature T_θ associated with the intra-chain coupling strength is about -346 K. However, no long-range magnetic order but a spin glass transition at ~3 K has been observed. Our results indicate that the spin glass behavior in Ba₉Co₃Se₁₅ mainly arises from the magnetic frustration due to the geometrically frustrated triangular lattice.

Key words: one-dimensional chain, spin glass, high-pressure

中图分类号: (X-ray diffraction)

61.05.cp

61.50.-f (Structure of bulk crystals) 61.66.Fn (Inorganic compounds) 61.82.Fk (Semiconductors)

段磊, 望贤成, 张俊, 赵建发, 曹立朋, 李文敏, 于润泽, 邓正, 靳常青. Synthesis, structure, and properties of Ba₉Co₃Se₁₅ with one-dimensional spin chains[J]. 中国物理B, 2020, 29(3): 36102-036102.

Lei Duan(段磊), Xian-Cheng Wang(望贤成), Jun Zhang(张俊), Jian-Fa Zhao(赵建发), Li-Peng Cao(曹立朋), Wen-Min Li(李文敏), Run-Ze Yu(于润泽), Zheng Deng(邓正), Chang-Qing Jin(靳常青). Synthesis, structure, and properties of Ba₉Co₃Se₁₅ with one-dimensional spin chains[J]. Chin. Phys. B, 2020, 29(3): 36102-036102.

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Synthesis, structure, and properties of Ba₉Co₃Se₁₅ with one-dimensional spin chains

Synthesis, structure, and properties of Ba₉Co₃Se₁₅ with one-dimensional spin chains

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