中国物理B ›› 2016, Vol. 25 ›› Issue (1): 18101-018101.doi: 10.1088/1674-1056/25/1/018101

• INTERDISCIPLINARY PHYSICS AND RELATED AREAS OF SCIENCE AND TECHNOLOGY • 上一篇    下一篇

Effect of fluence and ambient environment on the surface and structural modification of femtosecond laser irradiated Ti

Umm-i-Kalsoom, Shazia Bashir Nisar Ali, M Shahid Rafique, Wolfgang Husinsky, Chandra S R Nathala, Sergey V Makarov, Narjis Begum   

  1. 1. Institute for Applied Physics, Vienna University of Technology, Vienna, Austria;
    2. Centre for Advanced Studies in Physics, GC University Lahore, Pakistan;
    3. Department of Physics, The University of Lahore, Pakistan;
    4. Department of Basic Sciences and Humanities, University of Engineering and Technology Fasalabad, Pakistan;
    5. Department of Physics, University of Engineering and Technology Lahore, Pakistan;
    6. P. N. Lebedev Physics Institute RAS, Moscow, Russia;
    7. Department of Physics, COMSATS Institute of Information and Technology, Islamabad, Pakistan
  • 收稿日期:2015-05-16 修回日期:2015-08-27 出版日期:2016-01-05 发布日期:2016-01-05
  • 通讯作者: Umm-i-Kalsoom E-mail:ummikalsoom551@gmail.com
  • 基金资助:

    Project supported by Österreichische Forschungsfödergesellschaft (FFG) (Grant No. 834325).

Effect of fluence and ambient environment on the surface and structural modification of femtosecond laser irradiated Ti

Umm-i-Kalsoom1,2,3, Shazia Bashir2 Nisar Ali1,2,4, M Shahid Rafique5, Wolfgang Husinsky1, Chandra S R Nathala1, Sergey V Makarov6, Narjis Begum7   

  1. 1. Institute for Applied Physics, Vienna University of Technology, Vienna, Austria;
    2. Centre for Advanced Studies in Physics, GC University Lahore, Pakistan;
    3. Department of Physics, The University of Lahore, Pakistan;
    4. Department of Basic Sciences and Humanities, University of Engineering and Technology Fasalabad, Pakistan;
    5. Department of Physics, University of Engineering and Technology Lahore, Pakistan;
    6. P. N. Lebedev Physics Institute RAS, Moscow, Russia;
    7. Department of Physics, COMSATS Institute of Information and Technology, Islamabad, Pakistan
  • Received:2015-05-16 Revised:2015-08-27 Online:2016-01-05 Published:2016-01-05
  • Contact: Umm-i-Kalsoom E-mail:ummikalsoom551@gmail.com
  • Supported by:

    Project supported by Österreichische Forschungsfödergesellschaft (FFG) (Grant No. 834325).

摘要:

Under certain conditions, ultrafast pulsed laser interaction with matter leads to the formation of self-organized conical as well as periodic surface structures (commonly reffered to as, laser induced periodic surface structures, LIPSS). The purpose of the present investigations is to explore the effect of fsec laser fluence and ambient environments (Vacuum & O2) on the formation of LIPSS and conical structures on the Ti surface. The surface morphology was investigated by scanning electron microscope (SEM). The ablation threshold with single and multiple (N=100) shots and the existence of an incubation effect was demonstrated by SEM investigations for both the vacuum and the O2 environment. The phase analysis and chemical composition of the exposed targets were performed by x-ray diffraction (XRD) and energy dispersive x-ray spectroscopy (EDS), respectively. SEM investigations reveal the formation of LIPSS (nano & micro). FFT d-spacing calculations illustrate the dependence of periodicity on the fluence and ambient environment. The periodicity of nano-scale LIPSS is higher in the case of irradiation under vacuum conditions as compared to O2. Furthermore, the O2 environment reduces the ablation threshold. XRD data reveal that for the O2 environment, new phases (oxides of Ti) are formed. EDS analysis exhibits that after irradiation under vacuum conditions, the percentage of impurity element (Al) is reduced. The irradiation in the O2 environment results in 15% atomic diffusion of oxygen.

关键词: LIPSS, ablation threshold, incubation coefficient, structural modification

Abstract:

Under certain conditions, ultrafast pulsed laser interaction with matter leads to the formation of self-organized conical as well as periodic surface structures (commonly reffered to as, laser induced periodic surface structures, LIPSS). The purpose of the present investigations is to explore the effect of fsec laser fluence and ambient environments (Vacuum & O2) on the formation of LIPSS and conical structures on the Ti surface. The surface morphology was investigated by scanning electron microscope (SEM). The ablation threshold with single and multiple (N=100) shots and the existence of an incubation effect was demonstrated by SEM investigations for both the vacuum and the O2 environment. The phase analysis and chemical composition of the exposed targets were performed by x-ray diffraction (XRD) and energy dispersive x-ray spectroscopy (EDS), respectively. SEM investigations reveal the formation of LIPSS (nano & micro). FFT d-spacing calculations illustrate the dependence of periodicity on the fluence and ambient environment. The periodicity of nano-scale LIPSS is higher in the case of irradiation under vacuum conditions as compared to O2. Furthermore, the O2 environment reduces the ablation threshold. XRD data reveal that for the O2 environment, new phases (oxides of Ti) are formed. EDS analysis exhibits that after irradiation under vacuum conditions, the percentage of impurity element (Al) is reduced. The irradiation in the O2 environment results in 15% atomic diffusion of oxygen.

Key words: LIPSS, ablation threshold, incubation coefficient, structural modification

中图分类号:  (Sample preparation)

  • 06.60.Ei
06.60.Jn (High-speed techniques) 07.78.+s (Electron, positron, and ion microscopes; electron diffractometers) 07.85.Jy (Diffractometers)