中国物理B ›› 2024, Vol. 33 ›› Issue (9): 98104-098104.doi: 10.1088/1674-1056/ad58c6

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Pressure generation under deformation in a large-volume press

Saisai Wang(王赛赛)1,†, Xinyu Zhao(赵鑫宇)1,†, Kuo Hu(胡阔)1,‡, Bingtao Feng(丰丙涛)1, Xuyuan Hou(侯旭远)1, Yiming Zhang(张羿鸣)1, Shucheng Liu(刘书成)1, Yuchen Shang(尚宇琛)1,§, Zhaodong Liu(刘兆东)1,2,¶, Mingguang Yao(姚明光)1, and Bingbing Liu(刘冰冰)1   

  1. 1 State Key Laboratory of Superhard Materials, Synergetic Extreme Condition User Facility, College of Physics, Jilin University, Changchun 130012, China;
    2 College of Earth Sciences, Jilin University, Changchun 130012, China
  • 收稿日期:2024-04-18 修回日期:2024-06-06 接受日期:2024-06-17 发布日期:2024-08-22
  • 通讯作者: Kuo Hu, Yuchen Shang, Zhaodong Liu E-mail:hukuo@jlu.edu.cn;shangyc@jlu.edu.cn;liu_zhaodong@jlu.edu.cn
  • 基金资助:
    We acknowledge Yankun Yin for SEM analysis. Project supported by the National Natural Science Foundation of China (Grant Nos. 42272041, 41902034, 52302043, 12304015, 52302043, and 12011530063), the National Major Science Facility Synergetic Extreme Condition User Facility Achievement Transformation Platform Construction (Grant No. 2021FGWCXNLJSKJ01), the China Postdoctoral Science Foundation (Grant Nos. 2022M720054 and 2023T160257), the National Key Research and Development Program of China (Grant No. 2022YFB3706602), and the Jilin University High-level Innovation Team Foundation, China (Grant No. 2021TD-05).

Pressure generation under deformation in a large-volume press

Saisai Wang(王赛赛)1,†, Xinyu Zhao(赵鑫宇)1,†, Kuo Hu(胡阔)1,‡, Bingtao Feng(丰丙涛)1, Xuyuan Hou(侯旭远)1, Yiming Zhang(张羿鸣)1, Shucheng Liu(刘书成)1, Yuchen Shang(尚宇琛)1,§, Zhaodong Liu(刘兆东)1,2,¶, Mingguang Yao(姚明光)1, and Bingbing Liu(刘冰冰)1   

  1. 1 State Key Laboratory of Superhard Materials, Synergetic Extreme Condition User Facility, College of Physics, Jilin University, Changchun 130012, China;
    2 College of Earth Sciences, Jilin University, Changchun 130012, China
  • Received:2024-04-18 Revised:2024-06-06 Accepted:2024-06-17 Published:2024-08-22
  • Contact: Kuo Hu, Yuchen Shang, Zhaodong Liu E-mail:hukuo@jlu.edu.cn;shangyc@jlu.edu.cn;liu_zhaodong@jlu.edu.cn
  • Supported by:
    We acknowledge Yankun Yin for SEM analysis. Project supported by the National Natural Science Foundation of China (Grant Nos. 42272041, 41902034, 52302043, 12304015, 52302043, and 12011530063), the National Major Science Facility Synergetic Extreme Condition User Facility Achievement Transformation Platform Construction (Grant No. 2021FGWCXNLJSKJ01), the China Postdoctoral Science Foundation (Grant Nos. 2022M720054 and 2023T160257), the National Key Research and Development Program of China (Grant No. 2022YFB3706602), and the Jilin University High-level Innovation Team Foundation, China (Grant No. 2021TD-05).

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摘要： Deformation can change the transition pathway of materials under high pressure, thus significantly affects physical and chemical properties of matters. However, accurate pressure calibration under deformation is challenging and thereby causes relatively large pressure uncertainties in deformation experiments, resulting in the synthesis of complex multiphase materials. Here, pressure generations of three types of deformation assemblies were well calibrated in a Walker-type large-volume press (LVP) by electrical resistance measurements combined with finite element simulations (FESs). Hard Al$_{2}$O$_{3}$ or diamond pistons in shear and uniaxial deformation assemblies significantly increase the efficiency of pressure generation compared with the conventional quasi-hydrostatic assembly. The uniaxial deformation assembly using flat diamond pistons possesses the highest efficiency in these deformation assemblies. This finding is further confirmed by stress distribution analysis based on FESs. With this deformation assembly, we found shear can effectively promote the transformation of C$_{60}$ into diamond under high pressure and realized the synthesis of phase-pure diamond at relatively moderate pressure and temperature conditions. The present developed techniques will help improve pressure efficiencies in LVP and explore the new physical and chemical properties of materials under deformation in both science and technology.

关键词: shear/uniaxial deformation, pressure calibration, finite element simulations, large-volume press, high pressure

Abstract: Deformation can change the transition pathway of materials under high pressure, thus significantly affects physical and chemical properties of matters. However, accurate pressure calibration under deformation is challenging and thereby causes relatively large pressure uncertainties in deformation experiments, resulting in the synthesis of complex multiphase materials. Here, pressure generations of three types of deformation assemblies were well calibrated in a Walker-type large-volume press (LVP) by electrical resistance measurements combined with finite element simulations (FESs). Hard Al$_{2}$O$_{3}$ or diamond pistons in shear and uniaxial deformation assemblies significantly increase the efficiency of pressure generation compared with the conventional quasi-hydrostatic assembly. The uniaxial deformation assembly using flat diamond pistons possesses the highest efficiency in these deformation assemblies. This finding is further confirmed by stress distribution analysis based on FESs. With this deformation assembly, we found shear can effectively promote the transformation of C$_{60}$ into diamond under high pressure and realized the synthesis of phase-pure diamond at relatively moderate pressure and temperature conditions. The present developed techniques will help improve pressure efficiencies in LVP and explore the new physical and chemical properties of materials under deformation in both science and technology.

Key words: shear/uniaxial deformation, pressure calibration, finite element simulations, large-volume press, high pressure

中图分类号:  (Deformation, plasticity, and creep)

  • 81.40.Lm
07.35.+k (High-pressure apparatus; shock tubes; diamond anvil cells) 62.50.-p (High-pressure effects in solids and liquids) 81.40.Vw (Pressure treatment)