Properties of negative thermal expansion β-eucryptite ceramics prepared by spark plasma sintering

doi:10.1088/1674-1056/27/9/096501

中国物理B ›› 2018, Vol. 27 ›› Issue (9): 96501-096501.doi: 10.1088/1674-1056/27/9/096501

• CONDENSED MATTER: STRUCTURAL, MECHANICAL, AND THERMAL PROPERTIES • 上一篇下一篇

Properties of negative thermal expansion β-eucryptite ceramics prepared by spark plasma sintering

Li-Min Zhao(赵利敏), Yong-Guang Cheng(程永光), Hao-Shan Hao(郝好山), Jiao Wang(王娇), Shao-Hui Liu(刘少辉), Bao-Sen Zhang(张宝森)

School of Science, Henan Institute of Engineering, Zhengzhou 451191, China

收稿日期:2018-03-26 修回日期:2018-06-16 出版日期:2018-09-05 发布日期:2018-09-05
通讯作者: Hao-Shan Hao E-mail:hshhao@126.com
基金资助:
Project supported by the Programs for Tackling Key Problems in Science and Technology, Henan Province, China (Grant Nos. 172102210103, 182102310895, 182102210031, and 182102311079), the Doctoral Program of Henan Institute of Engineering, China (Grant Nos. D2016015 and D2016016), and the National-level College Students Innovative Entrepreneurial Training Plan Program, China (Grant No. 201611517041).

Properties of negative thermal expansion β-eucryptite ceramics prepared by spark plasma sintering

Li-Min Zhao(赵利敏), Yong-Guang Cheng(程永光), Hao-Shan Hao(郝好山), Jiao Wang(王娇), Shao-Hui Liu(刘少辉), Bao-Sen Zhang(张宝森)

School of Science, Henan Institute of Engineering, Zhengzhou 451191, China

Received:2018-03-26 Revised:2018-06-16 Online:2018-09-05 Published:2018-09-05
Contact: Hao-Shan Hao E-mail:hshhao@126.com
Supported by:
Project supported by the Programs for Tackling Key Problems in Science and Technology, Henan Province, China (Grant Nos. 172102210103, 182102310895, 182102210031, and 182102311079), the Doctoral Program of Henan Institute of Engineering, China (Grant Nos. D2016015 and D2016016), and the National-level College Students Innovative Entrepreneurial Training Plan Program, China (Grant No. 201611517041).

摘要/Abstract

摘要：

β-eucryptite powders are prepared by the sol-gel method through using tetraethoxysilane lithium nitrate and aluminum isopropoxide as starting materials. β-eucryptite ceramics are prepared by spark plasma sintering. The effects of sintering temperature on the negative thermal expansion properties of the β-eucryptite are investigated by x-ray diffraction (XRD), scanning electron microscopy, and thermal expansion test. The XRD results exhibit no change in the crystal structure of the sample prepared by different sintering processes. The negative thermal expansion properties increase with the increase of the sintering temperature. The coefficient of thermal expansion of β-eucryptite ceramics sintered at 1100 ℃ is calculated to be -4.93×10^-6 ℃^-1. Crystallization behaviors of the ceramics may play an important role in the increase of negative thermal expansion of β-eucryptite. High sintering temperature could improve the crystallization behaviors of the ceramics and reduce the residue glass phase, which can improve the negative thermal expansion properties of β-eucryptite ceramics.

关键词: β-eucryptite, thermal expansion, structure, spark plasma sintering

Abstract:

Key words: β-eucryptite, thermal expansion, structure, spark plasma sintering

中图分类号: (Thermal expansion; thermomechanical effects)

65.40.De

67.80.de (Structure, lattice dynamics and sound) 81.20.Ev (Powder processing: powder metallurgy, compaction, sintering, mechanical alloying, and granulation)

赵利敏, 程永光, 郝好山, 王娇, 刘少辉, 张宝森. Properties of negative thermal expansion β-eucryptite ceramics prepared by spark plasma sintering[J]. 中国物理B, 2018, 27(9): 96501-096501.

Li-Min Zhao(赵利敏), Yong-Guang Cheng(程永光), Hao-Shan Hao(郝好山), Jiao Wang(王娇), Shao-Hui Liu(刘少辉), Bao-Sen Zhang(张宝森). Properties of negative thermal expansion β-eucryptite ceramics prepared by spark plasma sintering[J]. Chin. Phys. B, 2018, 27(9): 96501-096501.

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Properties of negative thermal expansion β-eucryptite ceramics prepared by spark plasma sintering

Properties of negative thermal expansion β-eucryptite ceramics prepared by spark plasma sintering

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