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XRD AND EXAFS INVESTIGATION OF THE DECOMPOSITION OF Co-Cu SOLID SOLUTION PREPARED BY MELT SPINING
刘涛, 胡天斗, 谢亚宁, 蒋海音, 王德武, 王文东, 李华飚
1998 (7):
541-546.
doi: 10.1088/1004-423X/7/7/008
摘要
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1071 )
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High solid-solubility Co15Cu85 alloys were prepared by melt spining and then submitted to isothermal and anisothermal annealing to obtain granular alloys. The synchrotron radiation X-ray diffraction patterns and extended X-ray absorption fine structure (EXAFS) spectra were measured to investigate the decomposition of supersaturated solid solution upon annealing. Experimental results indicated the precipitation of ultrafine Co-rich particles occurred at about 500℃ and the annealing had a great influence on the middle-range order of Co atoms. While the fitted EXAFS spectra showed that the interfaces of Co precipitates seem to be enriched with vacancy-type defects, leading to distorted interfaces.
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