中国物理B ›› 2022, Vol. 31 ›› Issue (5): 56102-056102.doi: 10.1088/1674-1056/ac43aa

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Small-angle neutron scattering study on the stability of oxide nanoparticles in long-term thermally aged 9Cr-oxide dispersion strengthened steel

Peng-Lin Gao(高朋林)1,2, Jian Gong(龚建)2, Qiang Tian(田强)2, Gung-Ai Sun(孙光爱)2, Hai-Yang Yan(闫海洋)2, Liang Chen(陈良)2, Liang-Fei Bai(白亮飞)2, Zhi-Meng Guo(郭志猛)3, and Xin Ju(巨新)1,†   

  1. 1 Department of Physics, University of Science and Technology Beijing, Beijing 100083, China;
    2 Key Laboratory of Neutron Physics and Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang 621900, China;
    3 Institute of Power Metallurgy, University of Science and Technology Beijing, Beijing 100083, China
  • 收稿日期:2021-07-07 修回日期:2021-12-13 发布日期:2022-04-09
  • 通讯作者: Xin Ju,E-mail:jux@ustb.edu.cn E-mail:jux@ustb.edu.cn
  • 基金资助:
    Project supported by the National Key Research and Development Program of China (Grant No.2017YFB0702400).

Small-angle neutron scattering study on the stability of oxide nanoparticles in long-term thermally aged 9Cr-oxide dispersion strengthened steel

Peng-Lin Gao(高朋林)1,2, Jian Gong(龚建)2, Qiang Tian(田强)2, Gung-Ai Sun(孙光爱)2, Hai-Yang Yan(闫海洋)2, Liang Chen(陈良)2, Liang-Fei Bai(白亮飞)2, Zhi-Meng Guo(郭志猛)3, and Xin Ju(巨新)1,†   

  1. 1 Department of Physics, University of Science and Technology Beijing, Beijing 100083, China;
    2 Key Laboratory of Neutron Physics and Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang 621900, China;
    3 Institute of Power Metallurgy, University of Science and Technology Beijing, Beijing 100083, China
  • Received:2021-07-07 Revised:2021-12-13 Published:2022-04-09
  • Contact: Xin Ju,E-mail:jux@ustb.edu.cn E-mail:jux@ustb.edu.cn
  • About author:2021-12-16
  • Supported by:
    Project supported by the National Key Research and Development Program of China (Grant No.2017YFB0702400).

摘要: A 9Cr-oxide dispersion strengthened (ODS) steel was thermally aged at 873 K for up to 5000 h. The size distribution and chemical composition of the dispersed oxide nanoparticles were analyzed by small-angle neutron scattering under a magnetic field. Combined with transmission electron microscopy, Vickers micro-hardness tests and electron backscattered diffraction measurements, all the results showed that the thermal treatment had little or no effect on the size distributions and volume fractions of the oxide nanoparticles in the ferromagnetic matrix, which suggested excellent thermal stability of the 9Cr-ODS steel.

关键词: oxide dispersion strengthened (ODS) steel, small angle neutron scattering (SANS), thermal aging, nanoparticle

Abstract: A 9Cr-oxide dispersion strengthened (ODS) steel was thermally aged at 873 K for up to 5000 h. The size distribution and chemical composition of the dispersed oxide nanoparticles were analyzed by small-angle neutron scattering under a magnetic field. Combined with transmission electron microscopy, Vickers micro-hardness tests and electron backscattered diffraction measurements, all the results showed that the thermal treatment had little or no effect on the size distributions and volume fractions of the oxide nanoparticles in the ferromagnetic matrix, which suggested excellent thermal stability of the 9Cr-ODS steel.

Key words: oxide dispersion strengthened (ODS) steel, small angle neutron scattering (SANS), thermal aging, nanoparticle

中图分类号:  (Neutron scattering (including small-angle scattering))

  • 61.05.fg
68.37.Lp (Transmission electron microscopy (TEM)) 68.60.Dv (Thermal stability; thermal effects)