Photon-in/photon-out endstation for studies of energy materials at beamline 02B02 of Shanghai Synchrotron Radiation Facility

doi:10.1088/1674-1056/ab5d04

中国物理B ›› 2020, Vol. 29 ›› Issue (1): 16101-016101.doi: 10.1088/1674-1056/ab5d04

所属专题： SPECIAL TOPIC — Advanced calculation & characterization of energy storage materials & devices at multiple scale

• SPECIAL TOPIC—Recent advances in thermoelectric materials and devices • 上一篇下一篇

Photon-in/photon-out endstation for studies of energy materials at beamline 02B02 of Shanghai Synchrotron Radiation Facility

Guoxi Ren(任国玺), Nian Zhang(张念), Xuefei Feng(冯雪飞), Hui Zhang(章辉), Pengfei Yu(于鹏飞), Shun Zheng(郑顺), Deng Zhou(周櫈), Zongwang Tian(田宗旺), Xiaosong Liu(刘啸嵩)

1 State Key Laboratory of Functional Materials for Informatics, Shanghai Institute of Microsystem and Information Technology, Chinese Academy of Sciences, Shanghai 200050, China;
2 CAS Center for Excellence in Superconducting Electronics(CENSE), Chinese Academy of Sciences, Shanghai 200050, China;
3 University of Chinese Academy of Sciences, Beijing 100049, China;
4 School of Physical Science and Technology, Shanghai Tech University, Shanghai 201210, China

收稿日期:2019-10-30 修回日期:2019-11-15 出版日期:2020-01-05 发布日期:2020-01-05
通讯作者: Xiaosong Liu E-mail:xliu3@mail.sim.ac.cn
基金资助:
Project supported by the National Natural Science Foundation of China (Grant No. 11227902) as part of NSFC ME2 beamline project, Science and Technology Commission of Shanghai Municipality, China (Grant No. 14520722100), and the National Natural Science Foundation of China (Grant Nos. 11905283 and U1632269).

Photon-in/photon-out endstation for studies of energy materials at beamline 02B02 of Shanghai Synchrotron Radiation Facility

Guoxi Ren(任国玺)^1,2,3, Nian Zhang(张念)^1,2, Xuefei Feng(冯雪飞)^1,2, Hui Zhang(章辉)^1,2, Pengfei Yu(于鹏飞)^1,2, Shun Zheng(郑顺)^1,2,3, Deng Zhou(周櫈)^1,2,3, Zongwang Tian(田宗旺)^1,2,4, Xiaosong Liu(刘啸嵩)^1,2,4

1 State Key Laboratory of Functional Materials for Informatics, Shanghai Institute of Microsystem and Information Technology, Chinese Academy of Sciences, Shanghai 200050, China;
2 CAS Center for Excellence in Superconducting Electronics(CENSE), Chinese Academy of Sciences, Shanghai 200050, China;
3 University of Chinese Academy of Sciences, Beijing 100049, China;
4 School of Physical Science and Technology, Shanghai Tech University, Shanghai 201210, China

Received:2019-10-30 Revised:2019-11-15 Online:2020-01-05 Published:2020-01-05
Contact: Xiaosong Liu E-mail:xliu3@mail.sim.ac.cn
Supported by:
Project supported by the National Natural Science Foundation of China (Grant No. 11227902) as part of NSFC ME2 beamline project, Science and Technology Commission of Shanghai Municipality, China (Grant No. 14520722100), and the National Natural Science Foundation of China (Grant Nos. 11905283 and U1632269).

摘要/Abstract

摘要： A new photon-in/photon-out endstation at beamline 02B02 of the Shanghai Synchrotron Radiation Facility for studying the electronic structure of energy materials has been constructed and fully opened to users. The endstation has the capability to perform soft x-ray absorption spectroscopy in total electron yield and total fluorescence yield modes simultaneously. The photon energy ranges from 40 eV to 2000 eV covering the K-edge of most low Z-elements and the L-edge of 3d transition-metals. The new self-designed channeltron detector allows us to achieve good fluorescence signals at the low photon flux. In addition, we synchronously collect the signals of a standard reference sample and a gold mesh on the upstream to calibrate the photon energy and monitor the beam fluctuation, respectively. In order to cross the pressure gap, in situ gas and liquid cells for soft x-ray absorption spectroscopy are developed to study the samples under realistic working conditions.

关键词: soft x-ray absorption, energy materials, photon-in/photon-out, in situ cell

Abstract: A new photon-in/photon-out endstation at beamline 02B02 of the Shanghai Synchrotron Radiation Facility for studying the electronic structure of energy materials has been constructed and fully opened to users. The endstation has the capability to perform soft x-ray absorption spectroscopy in total electron yield and total fluorescence yield modes simultaneously. The photon energy ranges from 40 eV to 2000 eV covering the K-edge of most low Z-elements and the L-edge of 3d transition-metals. The new self-designed channeltron detector allows us to achieve good fluorescence signals at the low photon flux. In addition, we synchronously collect the signals of a standard reference sample and a gold mesh on the upstream to calibrate the photon energy and monitor the beam fluctuation, respectively. In order to cross the pressure gap, in situ gas and liquid cells for soft x-ray absorption spectroscopy are developed to study the samples under realistic working conditions.

Key words: soft x-ray absorption, energy materials, photon-in/photon-out, in situ cell

中图分类号: (X-ray absorption spectroscopy: EXAFS, NEXAFS, XANES, etc.)

61.05.cj

07.85.Qe (Synchrotron radiation instrumentation) 88.80.-q (Energy delivery and storage)

任国玺, 张念, 冯雪飞, 章辉, 于鹏飞, 郑顺, 周櫈, 田宗旺, 刘啸嵩. Photon-in/photon-out endstation for studies of energy materials at beamline 02B02 of Shanghai Synchrotron Radiation Facility[J]. 中国物理B, 2020, 29(1): 16101-016101.

Guoxi Ren(任国玺), Nian Zhang(张念), Xuefei Feng(冯雪飞), Hui Zhang(章辉), Pengfei Yu(于鹏飞), Shun Zheng(郑顺), Deng Zhou(周櫈), Zongwang Tian(田宗旺), Xiaosong Liu(刘啸嵩). Photon-in/photon-out endstation for studies of energy materials at beamline 02B02 of Shanghai Synchrotron Radiation Facility[J]. Chin. Phys. B, 2020, 29(1): 16101-016101.

参考文献 29

[1]	Etacheri V, Marom R, Elazari R, Salitra G and Aurbach D 2011 Energ. Environ Sci. 4 3243 doi: 10.1039/c1ee01598b
[2]	Cheng X B, Zhang R, Zhao C Z and Zhang Q 2017 Chem. Rev. 117 10403 doi: 10.1021/acs.chemrev.7b00115
[3]	Mefford J T, Rong X, Abakumov A M, Hardin W G, Dai S, Kolpak A M, Johnston K P and Stevenson K J 2016 Nat. Commun. 7 11053 doi: 10.1038/ncomms11053
[4]	Sun M H, Huang S Z, Chen L H, Li Y, Yang X Y, Yuan Z Y and Su B L 2016 Chem. Soc. Rev. 45 3479 doi: 10.1039/C6CS00135A
[5]	Yu H S, Wei X J, Li J, Gu S Q, Zhang S, Wang L H, Ma J Y, Li L N, Gao Q, Si R, Sun F F, Wang Y, Song F, Xu H J, Yu X H, Zou Y, Wang J Q, Jiang Z and Huang Y Y 2015 Nucl. Sci. Tech. 26 050102
[6]	Cai J, Dong Q, Han Y, Mao B H, Zhang H, Karlsson P G, Åhlund J, Tai R Z, Yu Y and Liu Z 2019 Nucl. Sci. Tech. 30 81 doi: 10.1007/s41365-019-0608-0
[7]	Zheng L and Wu X S 2013 Chin. Phys. B 22 107806 doi: 10.1088/1674-1056/22/10/107806
[8]	Long X H, Wu Y R, Zhang N, Yu P F, Feng X F, Zheng S, Fu J M, Liu X S, Liu N, Wang M, Xu L M, Chen J M and Lee J M 2018 Chin. Phys. B 27 107802 doi: 10.1088/1674-1056/27/10/107802
[9]	Zhang N, Long X H, Wang Z, Yu P F, Han F D, Fu J M, Ren G X, Wu Y R, Zheng S, Huang W C, Wang C S, Li H and Liu X S 2018 ACS Appl. Energy Mater. 1 5968 doi: 10.1021/acsaem.8b01035
[10]	Moses A W, Flores H G G, Kim J G and Langell M A 2007 Appl. Surf. Sci. 253 4782 doi: 10.1016/j.apsusc.2006.10.044
[11]	Qiao R M, Wray L A, Kim J H, Pieczonka N P W, Harris S J and Yang W L 2015 J. Phys. Chem. C 119 27228 doi: 10.1021/acs.jpcc.5b07479
[12]	Wan G, Yu P F, Chen H R, Wen J G, Sun C J, Zhou H, Zhang N, Li Q R, Zhao W P, Xie B, Li T and Shi J L 2018 Small 14 e1704319
[13]	Fu J M, Yu P F, Zhang N, Ren G X, Zheng S, Huang W C, Long X H, Li H and Liu X S 2019 Energ. Environ Sci. 12 1404 doi: 10.1039/C8EE03390K
[14]	Qiao R M, Lucas I T, Karim A, Syzdek J, Liu X S, Chen W, Persson K, Kostecki R and Yang W L 2014 Adv. Mater. Interfaces 1 1300115 doi: 10.1002/admi.201300115
[15]	Liu X S, Wang D D, Liu G, Srinivasan V, Liu Z, Hussain Z and Yang W L 2013 Nat. Commun. 4 2568 doi: 10.1038/ncomms3568
[16]	Rao F, Song Z T, Cheng Y, Liu X S, Xia M J, Li W, Ding K Y, Feng X F, Zhu M and Feng S L 2015 Nat. Commun. 6 10040 doi: 10.1038/ncomms10040
[17]	Zhang S, Gu S Q, Wang Y, Liang C, Yu Y, Han L, Zheng S, Zhang N, Liu X S, Zhou J and Li J 2019 ACS Catal 9 7389 doi: 10.1021/acscatal.9b00928
[18]	Yang J, Qiu Z Y, Zhao C M, Wei W C, Chen W X, Li Z J, Qu Y T, Dong J C, Luo J, Li Z Y and Wu Y E 2018 Angew. Chem. Int. Ed. Engl. 57 14095 doi: 10.1002/anie.201808049
[19]	Wan J W, Chen W X, Jia C Y, Zheng L R, Dong J C, Zheng X S, Wang Y, Yan W S, Chen C, Peng Q, Wang D S and Li Y D 2018 Adv. Mater. 30 1705369 doi: 10.1002/adma.201705369
[20]	Yu M J, Wang Y and Xu W 2016 Chin. Phys. B 25 048701 doi: 10.1088/1674-1056/25/4/048701
[21]	Yang J, Zhu F, Zhang Q, Wu Y, Wu X, Qin S, Dong J C and Chen D L 2013 Chin. Phys. Lett. 30 046101 doi: 10.1088/0256-307X/30/4/046101
[22]	Yu P F, Cui Z H, Meng J W and Guo X X 2013 Chin. Phys. Lett. 30 036102 doi: 10.1088/0256-307X/30/3/036102
[23]	Meng X Y, Guo Z, Wang Y, Zhang H, Han Y, Zhao G F, Liu Z and Tai R Z 2019 J. Synchrotron Radiat 26 543 doi: 10.1107/S1600577518018179
[24]	Guo Z, Meng X Y, Wang Y, Liu H G, Zhang X Z, Li Z L, Xue L and Tai R Z 2017 J. Synchrotron Radiat 24 877 doi: 10.1107/S1600577517006087
[25]	Guo J H, Luo Y, Augustsson A, Rubensson J E, Sathe C, Agren H, Siegbahn H and Nordgren J 2002 Phys. Rev. Lett. 89 137402 doi: 10.1103/PhysRevLett.89.137402
[26]	Guo J H 2013 J. Electron. Spectrosc. Relat. Phenom. 188 71 doi: 10.1016/j.elspec.2012.12.007
[27]	Arthur T S, Glans P A, Matsui M, Zhang R G, Ma B W and Guo J H 2012 Electrochem. Commun. 24 43 doi: 10.1016/j.elecom.2012.08.018
[28]	Liu X S, Liu J, Qiao R M, Yu Y, Li H, Suo L M, Hu Y S, Chuang Y D, Shu G J, Chou F C, Weng T C, Nordlund D, Sokaras D, Wang Y J, Lin H, Barbiellini B, Bansil A, Song X Y, Liu Z, Yan S S, Liu G, Qiao S, Richardson T J, Prendergast D, Hussain Z, de Groot F M F and Yang W L 2012 J. Am. Chem. Soc. 134 13708 doi: 10.1021/ja303225e
[29]	Cheng L, Crumlin E J, Chen W, Qiao R M, Hou H M, Franz Lux S, Zorba V, Russo R, Kostecki R, Liu Z, Persson K, Yang W L, Cabana J, Richardson T, Chen G Y and Doeff M 2014 Phys. Chem. Chem. Phys. 16 18294 doi: 10.1039/C4CP02921F

Photon-in/photon-out endstation for studies of energy materials at beamline 02B02 of Shanghai Synchrotron Radiation Facility

Photon-in/photon-out endstation for studies of energy materials at beamline 02B02 of Shanghai Synchrotron Radiation Facility

RichHTML

PDF (PC)

赞

可视化

摘要/Abstract

引用本文

使用本文

参考文献 29

相关文章 1

Metrics

本文评价

推荐阅读 0