Structural transitions in NaNH2 via recrystallization under high pressure

doi:10.1088/1674-1056/ab37f8

中国物理B ›› 2019, Vol. 28 ›› Issue (9): 96402-096402.doi: 10.1088/1674-1056/ab37f8

• CONDENSED MATTER: STRUCTURAL, MECHANICAL, AND THERMAL PROPERTIES • 上一篇下一篇

Structural transitions in NaNH₂ via recrystallization under high pressure

Yanping Huang(黄艳萍), Xiaoli Haung(黄晓丽), Xin Wang(王鑫), Wenting Zhang(张文亭), Di Zhou(周迪), Qiang Zhou(周强), Bingbing Liu(刘冰冰), Tian Cui(崔田)

College of Physics, State Key Laboratory of Superhard Materials, Jilin University, Changchun 130012, China

收稿日期:2019-05-28 修回日期:2019-07-10 出版日期:2019-09-05 发布日期:2019-09-05
通讯作者: Yanping Huang, Xiaoli Haung, Xin Wang E-mail:huangyp1124@jlu.edu.cn;huangxiaoli@jlu.edu.cn;huangxiaoli@jlu.edu.cn
基金资助:
Project supported by the National Key R&D Program of China (Grant Nos. 2018YFA0305900 and 2016YFB0201204), the National Natural Science Foundation of China (Grant Nos. 51632002, 51572108, 11504127, 91745203, and 11634004), Program for Changjiang Scholars and Innovative Research Team in University, China (Grant No. IRT_15R23), and National Fund for Fostering Talents of Basic Science, China (Grant No. J1103202).

Structural transitions in NaNH₂ via recrystallization under high pressure

Yanping Huang(黄艳萍), Xiaoli Haung(黄晓丽), Xin Wang(王鑫), Wenting Zhang(张文亭), Di Zhou(周迪), Qiang Zhou(周强), Bingbing Liu(刘冰冰), Tian Cui(崔田)

College of Physics, State Key Laboratory of Superhard Materials, Jilin University, Changchun 130012, China

Received:2019-05-28 Revised:2019-07-10 Online:2019-09-05 Published:2019-09-05
Contact: Yanping Huang, Xiaoli Haung, Xin Wang E-mail:huangyp1124@jlu.edu.cn;huangxiaoli@jlu.edu.cn;huangxiaoli@jlu.edu.cn
Supported by:
Project supported by the National Key R&D Program of China (Grant Nos. 2018YFA0305900 and 2016YFB0201204), the National Natural Science Foundation of China (Grant Nos. 51632002, 51572108, 11504127, 91745203, and 11634004), Program for Changjiang Scholars and Innovative Research Team in University, China (Grant No. IRT_15R23), and National Fund for Fostering Talents of Basic Science, China (Grant No. J1103202).

摘要/Abstract

摘要：

Multiple phase transitions are detected in sodium amide (NaNH₂), an important hydrogen storage material, upon compression in diamond anvil cells (DAC) by using Raman spectroscopy and x-ray diffraction (XRD) measurements. Additional Bragg reflections appear on lower and higher angle sides of the original ones at~1.07 GPa and 1.84 GPa, accompanied by obvious changes in Raman spectroscopy, respectively. It reveals that NaNH₂ undergoes the high-pressure phase sequence (α-β-γ) up to 20 GPa at room temperature. Spectral analysis indicates an orthorhombic structure with PBAN space group for the γ phase. We also experimentally observe high pressure induced recrystallization in alkaline amide compounds for the first time.

关键词: high pressure, sodium amide, phase transition, recrystallization

Abstract:

Key words: high pressure, sodium amide, phase transition, recrystallization

中图分类号: (General studies of phase transitions)

64.60.-i

07.35.+k (High-pressure apparatus; shock tubes; diamond anvil cells) 61.05.cp (X-ray diffraction) 78.30.-j (Infrared and Raman spectra)

黄艳萍, 黄晓丽, 王鑫, 张文亭, 周迪, 周强, 刘冰冰, 崔田. Structural transitions in NaNH₂ via recrystallization under high pressure[J]. 中国物理B, 2019, 28(9): 96402-096402.

Yanping Huang(黄艳萍), Xiaoli Haung(黄晓丽), Xin Wang(王鑫), Wenting Zhang(张文亭), Di Zhou(周迪), Qiang Zhou(周强), Bingbing Liu(刘冰冰), Tian Cui(崔田). Structural transitions in NaNH₂ via recrystallization under high pressure[J]. Chin. Phys. B, 2019, 28(9): 96402-096402.

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Structural transitions in NaNH₂ via recrystallization under high pressure

Structural transitions in NaNH₂ via recrystallization under high pressure

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