In-situ ultrasonic calibrations of pressure and temperature in a hinge-type double-stage cubic large volume press

doi:10.1088/1674-1056/ac4902

中国物理B ›› 2022, Vol. 31 ›› Issue (6): 60702-060702.doi: 10.1088/1674-1056/ac4902

In-situ ultrasonic calibrations of pressure and temperature in a hinge-type double-stage cubic large volume press

Qingze Li(李青泽), Xiping Chen(陈喜平), Lei Xie(谢雷), Tiexin Han(韩铁鑫), Jiacheng Sun(孙嘉程), and Leiming Fang(房雷鸣)^†

Key Laboratory for Neutron Physics, Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang 621900, China

收稿日期:2021-11-02 修回日期:2021-12-27 接受日期:2022-01-07 出版日期:2022-05-17 发布日期:2022-05-19
通讯作者: Leiming Fang E-mail:flmyaya2008@163.com
基金资助:
Project supported by the National Natural Science Foundation of China (Grant Nos. 12075215, 11872198, and U2030110) and the National Key Research and Development Program of China (Grant No. 2016YFA0401503).

In-situ ultrasonic calibrations of pressure and temperature in a hinge-type double-stage cubic large volume press

Qingze Li(李青泽), Xiping Chen(陈喜平), Lei Xie(谢雷), Tiexin Han(韩铁鑫), Jiacheng Sun(孙嘉程), and Leiming Fang(房雷鸣)^†

Key Laboratory for Neutron Physics, Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang 621900, China

Received:2021-11-02 Revised:2021-12-27 Accepted:2022-01-07 Online:2022-05-17 Published:2022-05-19
Contact: Leiming Fang E-mail:flmyaya2008@163.com
Supported by:
Project supported by the National Natural Science Foundation of China (Grant Nos. 12075215, 11872198, and U2030110) and the National Key Research and Development Program of China (Grant No. 2016YFA0401503).

摘要/Abstract

摘要： Here, simultaneous in-situ calibration of pressures and temperatures was performed in a hinge-type second-stage cubic large volume press (LVP) up to 15 GPa and 1400 K by an acoustic travel-time approach. Based on the recently reported P-t_S and P-T-t_P-t_S equations for Al₂O₃ buffer rod, the cell pressures and temperatures in the chamber of LVP were in-situ determined, in comparison with those by conventional off-line (or fixed-points) pressure calibration method and direct thermocouple measurement, respectively. It is found that the cell pressures of the LVP chamber are significantly reduced after annealing at simultaneous high pressures and high temperatures, owing to the stress relaxation as accumulate in the LVP chamber. This acoustic travel-time method is verified to be a good way for precise determination of thermal (cell) pressures at high temperature conditions, and is of great importance and necessity to conduct in-situ physical property measurements under extreme high P-T conditions, especially when the precious synchrotron x-ray/neutron diffraction beams are not available.

关键词: cubic press, simultaneous in-situ calibration of pressures and temperatures, acoustic travel-time, high pressure and high temperature

Abstract: Here, simultaneous in-situ calibration of pressures and temperatures was performed in a hinge-type second-stage cubic large volume press (LVP) up to 15 GPa and 1400 K by an acoustic travel-time approach. Based on the recently reported P-t_S and P-T-t_P-t_S equations for Al₂O₃ buffer rod, the cell pressures and temperatures in the chamber of LVP were in-situ determined, in comparison with those by conventional off-line (or fixed-points) pressure calibration method and direct thermocouple measurement, respectively. It is found that the cell pressures of the LVP chamber are significantly reduced after annealing at simultaneous high pressures and high temperatures, owing to the stress relaxation as accumulate in the LVP chamber. This acoustic travel-time method is verified to be a good way for precise determination of thermal (cell) pressures at high temperature conditions, and is of great importance and necessity to conduct in-situ physical property measurements under extreme high P-T conditions, especially when the precious synchrotron x-ray/neutron diffraction beams are not available.

Key words: cubic press, simultaneous in-situ calibration of pressures and temperatures, acoustic travel-time, high pressure and high temperature

中图分类号: (High-pressure apparatus; shock tubes; diamond anvil cells)

07.35.+k

91.60.Gf (High-pressure behavior) 91.60.Lj (Acoustic properties) 43.35.Yb (Ultrasonic instrumentation and measurement techniques)

Qingze Li(李青泽), Xiping Chen(陈喜平), Lei Xie(谢雷), Tiexin Han(韩铁鑫), Jiacheng Sun(孙嘉程), and Leiming Fang(房雷鸣). In-situ ultrasonic calibrations of pressure and temperature in a hinge-type double-stage cubic large volume press[J]. 中国物理B, 2022, 31(6): 60702-060702.

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In-situ ultrasonic calibrations of pressure and temperature in a hinge-type double-stage cubic large volume press

In-situ ultrasonic calibrations of pressure and temperature in a hinge-type double-stage cubic large volume press

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