Synthesis of black phosphorus structured polymeric nitrogen

doi:10.1088/1674-1056/aba9bd

中国物理B ›› 2020, Vol. 29 ›› Issue (10): 106201-.doi: 10.1088/1674-1056/aba9bd

Ying Liu(刘影)¹^,†(), Haipeng Su(苏海鹏)¹, Caoping Niu(牛草萍)²^,³, Xianlong Wang(王贤龙)²^,³, Junran Zhang(张俊然)⁴, Zhongxue Ge(葛忠学)¹, Yanchun Li(李延春)⁴

收稿日期:2020-06-23 修回日期:2020-07-16 接受日期:2020-07-28 出版日期:2020-10-05 发布日期:2020-10-05
通讯作者: Ying Liu(刘影)

Synthesis of black phosphorus structured polymeric nitrogen

Ying Liu(刘影)^1,†, Haipeng Su(苏海鹏)¹, Caoping Niu(牛草萍)^2,3,, Xianlong Wang(王贤龙)^2,3, Junran Zhang(张俊然)⁴, Zhongxue Ge(葛忠学)¹, and Yanchun Li(李延春)⁴

¹ Xi’an Modern Chemistry Research Institute, Xi’an 710065, China
² Key Laboratory of Materials Physics, Institute of Solid State Physics, HFIPS, Chinese Academy of Sciences, Hefei 230031, China
³ University of Science and Technology of China, Hefei 230026, China
⁴ Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049, China

Received:2020-06-23 Revised:2020-07-16 Accepted:2020-07-28 Online:2020-10-05 Published:2020-10-05
Contact: ^†Corresponding author. E-mail: liuying8912@aliyun.com
About author:
†Corresponding author. E-mail: liuying8912@aliyun.com
* Project supported by the National Natural Science Foundation of China (Grant No. 11904281).

摘要/Abstract

Abstract:

Since the discoveries of polymeric nitrogen, named cg-N (2004), LP-N (2014), HLP-N (2019), another polymorph named black phosphorus nitrogen (BP-N) was synthesized at high-pressure-high-temperature conditions. The narrow existing pressure region and similar synthesized pressure of BP-N compared with cg-N indicate that the stable energy and enthalpy of formation of these two structures are close to each other, which was confirmed by our theoretical calculation. In order to obtain the pressure region of BP-N phase, pure N₂ and TiN/Pb + N₂ precursors were used for laser-heating high pressure experiments in diamond anvil cell (DAC), and the phase identity was examined by Raman and XRD mapping. BP-N can be synthesized in the pressure range of 130 GPa to 140 GPa with the assistance of heating absorber. With the decrease of the pressure, BP-N can be quenched to ∼ 40 GPa. The synthesizing pressure–temperature and the stable pressure region of BP-N are important for further exploration of BP-N and its kinetic and thermal dynamic relationship with other polymeric nitrogen, especially cg-N.

Key words: high pressure and high temperature, energetic materials, polymeric nitrogen, diamond anvil cell

中图分类号: (High-pressure effects in solids and liquids)

62.50.-p

61.05.cp (X-ray diffraction) 42.62.-b (Laser applications) 07.35.+k (High-pressure apparatus; shock tubes; diamond anvil cells)

Ying Liu(刘影), Haipeng Su(苏海鹏), Caoping Niu(牛草萍), Xianlong Wang(王贤龙), Junran Zhang(张俊然), Zhongxue Ge(葛忠学), Yanchun Li(李延春). [J]. 中国物理B, 2020, 29(10): 106201-.

Ying Liu(刘影)†, Haipeng Su(苏海鹏), Caoping Niu(牛草萍), Xianlong Wang(王贤龙), Junran Zhang(张俊然), Zhongxue Ge(葛忠学), and Yanchun Li(李延春). Synthesis of black phosphorus structured polymeric nitrogen[J]. Chin. Phys. B, 2020, 29(10): 106201-.

图/表 5

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#	Pressure/GPa	Temperature/K	Absorber	Results
I	∼ 143	∼ 2500	–	BP-N
II	∼ 130	∼ 1800	–	cg-N
III	∼ 130	∼ 2500	TiN	BP-N
IV	∼ 130	∼ 2500	Pb	BP-N
V	∼ 120	∼ 2500	TiN	–

Synthesis of black phosphorus structured polymeric nitrogen

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