Effects of helium irradiation dose and temperature on the damage evolution of Ti3SiC2 ceramic

doi:10.1088/1674-1056/28/7/076104

中国物理B ›› 2019, Vol. 28 ›› Issue (7): 76104-076104.doi: 10.1088/1674-1056/28/7/076104

• CONDENSED MATTER: STRUCTURAL, MECHANICAL, AND THERMAL PROPERTIES • 上一篇下一篇

Effects of helium irradiation dose and temperature on the damage evolution of Ti₃SiC₂ ceramic

Hua-Hai Shen(申华海), Xia Xiang(向霞), Hai-Bin Zhang(张海斌), Xiao-Song Zhou(周晓松), Hong-Xiang Deng(邓洪祥), Xiao-Tao Zu(祖小涛)

1 Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang 621900, China;
2 School of Physics, University of Electronic Science and Technology of China, Chengdu 610054, China

收稿日期:2019-03-14 修回日期:2019-04-08 出版日期:2019-07-05 发布日期:2019-07-05
通讯作者: Hua-Hai Shen, Hong-Xiang Deng E-mail:huahaishen@caep.cn;denghx@uestc.edu.cn
基金资助:
Project supported by the President Foundation of the China Academy of Engineering Physics (Grant No. YZJJLX2018003) and the National Natural Science Foundation of China (Grant No. 21601168).

Effects of helium irradiation dose and temperature on the damage evolution of Ti₃SiC₂ ceramic

Hua-Hai Shen(申华海)¹, Xia Xiang(向霞)², Hai-Bin Zhang(张海斌)¹, Xiao-Song Zhou(周晓松)¹, Hong-Xiang Deng(邓洪祥)², Xiao-Tao Zu(祖小涛)²

1 Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang 621900, China;
2 School of Physics, University of Electronic Science and Technology of China, Chengdu 610054, China

Received:2019-03-14 Revised:2019-04-08 Online:2019-07-05 Published:2019-07-05
Contact: Hua-Hai Shen, Hong-Xiang Deng E-mail:huahaishen@caep.cn;denghx@uestc.edu.cn
Supported by:
Project supported by the President Foundation of the China Academy of Engineering Physics (Grant No. YZJJLX2018003) and the National Natural Science Foundation of China (Grant No. 21601168).

摘要/Abstract

摘要：

The effects of 400 keV helium ion irradiation dose and temperature on the microstructure of the Ti₃SiC₂ ceramic were systematically investigated by grazing incidence x-ray diffraction, scanning electron microscopy, and transmission electron microscopy. The helium irradiation experiments were performed at both room temperature (RT) and 500 °C with a fluence up to 2.0×10¹⁷ He⁺/cm² that resulted in a maximum damage of 9.6 displacements per atom. Our results demonstrate that He irradiations produce a large number of nanometer defects in Ti₃SiC₂ lattice and then cause the dissociation of Ti₃SiC₂ to TiC nano-grains with the increasing He fluence. Irradiation induced cell volume swelling of Ti₃SiC₂ at RT is slightly higher than that at 500 °C, suggesting that Ti₃SiC₂ is more suitable for use in a high temperature environment. The temperature dependence of cell parameter evolution and the aggregation of He bubbles in Ti₃SiC₂ are different from those in Ti₃AlC₂. The formation of defects and He bubbles at the projected depth would induce the degradation of mechanical performance.

关键词: MAX, Ti₃SiC₂, helium irradiation, He bubble

Abstract:

Key words: MAX, Ti₃SiC₂, helium irradiation, He bubble

中图分类号: (Techniques for structure determination)

61.05.-a

61.05.J- (Electron diffraction and scattering) 61.80.Lj (Atom and molecule irradiation effects) 81.05.Je (Ceramics and refractories (including borides, carbides, hydrides, nitrides, oxides, and silicides))

申华海, 向霞, 张海斌, 周晓松, 邓洪祥, 祖小涛. Effects of helium irradiation dose and temperature on the damage evolution of Ti₃SiC₂ ceramic[J]. 中国物理B, 2019, 28(7): 76104-076104.

Hua-Hai Shen(申华海), Xia Xiang(向霞), Hai-Bin Zhang(张海斌), Xiao-Song Zhou(周晓松), Hong-Xiang Deng(邓洪祥), Xiao-Tao Zu(祖小涛). Effects of helium irradiation dose and temperature on the damage evolution of Ti₃SiC₂ ceramic[J]. Chin. Phys. B, 2019, 28(7): 76104-076104.

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Effects of helium irradiation dose and temperature on the damage evolution of Ti₃SiC₂ ceramic

Effects of helium irradiation dose and temperature on the damage evolution of Ti₃SiC₂ ceramic

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