High pressure x-ray diffraction techniques with synchrotron radiation

doi:10.1088/1674-1056/25/7/076106

Abstract

This article summarizes the developments of experimental techniques for high pressure x-ray diffraction (XRD) in diamond anvil cells (DACs) using synchrotron radiation. Basic principles and experimental methods for various diffraction geometry are described, including powder diffraction, single crystal diffraction, radial diffraction, as well as coupling with laser heating system. Resolution in d-spacing of different diffraction modes is discussed. More recent progress, such as extended application of single crystal diffraction for measurements of multigrain and electron density distribution, time-resolved diffraction with dynamic DAC and development of modulated heating techniques are briefly introduced. The current status of the high pressure beamline at BSRF (Beijing Synchrotron Radiation Facility) and some results are also presented.

Keywords: high pressure x-ray diffraction synchrotron radiation diamond anvil cell

Received: 04 March 2016
Accepted manuscript online:

PACS:	61.05.cp	(X-ray diffraction)
	07.35.+k	(High-pressure apparatus; shock tubes; diamond anvil cells)
	07.85.Qe	(Synchrotron radiation instrumentation)
	07.20.Ka	(High-temperature instrumentation; pyrometers)

Fund:

Project supported by the National Natural Science Foundation of China (Grant Nos. 10875142, 11079040, and 11075175). The 4W2 beamline of BSRF was supported by the Chinese Academy of Sciences (Grant Nos. KJCX2-SW-N20, KJCX2-SW-N03, and SYGNS04).

Corresponding Authors: Jing Liu
E-mail: liuj@ihep.ac.cn

Cite this article:

Jing Liu(刘景) High pressure x-ray diffraction techniques with synchrotron radiation 2016 Chin. Phys. B 25 076106

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