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Chin. Phys. B, 2018, Vol. 27(5): 054216    DOI: 10.1088/1674-1056/27/5/054216
ELECTROMAGNETISM, OPTICS, ACOUSTICS, HEAT TRANSFER, CLASSICAL MECHANICS, AND FLUID DYNAMICS Prev   Next  

Structural, vibrational, optical, photoluminescence, thermal, dielectric, and mechanical studies on zinc (tris) thiourea sulfate single crystal: A noticeable effect of organic dye

Mohd Shkir1, V Ganesh1, S AlFaify1, I S Yahia1, Mohd Anis2
1 Advanced Functional Materials & Optoelectronic Laboratory, Department of Physics, Faculty of Science, King Khalid University, Abha 61413, Saudi Arabia;
2 Department of Physics, Sant Gadge Baba Amravati University, Amravati 444602, Maharashtra, India
Abstract  In this work, uranine-dyed zinc (tris) thiourea sulfate (ZTS) monocrystals, 26 mm×15 mm×10 mm in size, were synthesized by the solution method at ambient temperature. Their purity, crystallinity, lattice parameters, and functional modes were studied by x-ray diffraction, Fourier transform-infrared spectroscopy (FT-IR), and FT-Raman spectroscopy analyses. The sodium ion content of the crystals from the dye was confirmed by elemental analysis. The diffused reflectance spectral analysis of the dyed crystal revealed a characteristic absorption band at 490 nm attributed to the presence of the dye. The calculated band gaps of the non-dyed and dyed crystals were 4.53 and 4.57 eV, respectively. A green emission peak at ~(512±4) nm was observed in the photoluminescence spectrum of the uranine-dyed crystals. A differential scanning calorimetry study confirmed that the thermal stability improved owing to the addition of the dye. Dielectric and microhardness studies were conducted to examine the significant improvements in the corresponding properties of dyed crystals. The results demonstrated the competency of the dyed ZTS crystals for applications in optoelectronic devices.
Keywords:  crystal growth      dielectric properties      luminescence      thermal properties      mechanical properties  
Received:  07 December 2017      Revised:  22 January 2018      Accepted manuscript online: 
PACS:  42.70.Mp (Nonlinear optical crystals)  
  77.84.-s (Dielectric, piezoelectric, ferroelectric, and antiferroelectric materials)  
  42.72.Bj (Visible and ultraviolet sources)  
  74.25.Jb (Electronic structure (photoemission, etc.))  
Fund: Project supported by the Fund from the Deanship of Scientific Research at King Khalid University,Saudi Arabia (Grant No.R.G.P.2/9/38).
Corresponding Authors:  Mohd Shkir, S AlFaify     E-mail:  shkirphysics@gmail.com;sasaalfaify@hotmail.com

Cite this article: 

Mohd Shkir, V Ganesh, S AlFaify, I S Yahia, Mohd Anis Structural, vibrational, optical, photoluminescence, thermal, dielectric, and mechanical studies on zinc (tris) thiourea sulfate single crystal: A noticeable effect of organic dye 2018 Chin. Phys. B 27 054216

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