Crystallization and characteristics of {100}-oriented diamond with CH4N2S additive under high pressure and high temperature

doi:10.1088/1674-1056/ab99b9

中国物理B ›› 2020, Vol. 29 ›› Issue (9): 98103-098103.doi: 10.1088/1674-1056/ab99b9

Crystallization and characteristics of {100}-oriented diamond with CH₄N₂S additive under high pressure and high temperature

Yong Li(李勇), Debing Tan(谭德斌), Qiang Wang(王强), Zhengguo Xiao(肖政国), Changhai Tian(田昌海), Lin Chen(陈琳)

Department of Physics and Electrical Engineering, Tongren University, Tongren 554300, China

收稿日期:2020-05-06 修回日期:2020-05-28 接受日期:2020-06-05 出版日期:2020-09-05 发布日期:2020-09-05
通讯作者: Yong Li E-mail:likaiyong6@163.com
基金资助:
Project supported by the National Natural Science Foundation of China (Grant No. 11604246), Natural Science Foundation of Guizhou Province Education Department of China (Grant Nos. KY2017053 and KY2018343), Natural Science Foundation of Guizhou Procince Science and Technology Agency of China (Grant Nos. 20181163 and LH 20177311), and Outstanding Young Science and Technology Talents of Guizhou Pronice of China (Grant No. 20195673).

Crystallization and characteristics of {100}-oriented diamond with CH₄N₂S additive under high pressure and high temperature

Yong Li(李勇), Debing Tan(谭德斌), Qiang Wang(王强), Zhengguo Xiao(肖政国), Changhai Tian(田昌海), Lin Chen(陈琳)

Department of Physics and Electrical Engineering, Tongren University, Tongren 554300, China

Received:2020-05-06 Revised:2020-05-28 Accepted:2020-06-05 Online:2020-09-05 Published:2020-09-05
Contact: Yong Li E-mail:likaiyong6@163.com
Supported by:
Project supported by the National Natural Science Foundation of China (Grant No. 11604246), Natural Science Foundation of Guizhou Province Education Department of China (Grant Nos. KY2017053 and KY2018343), Natural Science Foundation of Guizhou Procince Science and Technology Agency of China (Grant Nos. 20181163 and LH 20177311), and Outstanding Young Science and Technology Talents of Guizhou Pronice of China (Grant No. 20195673).

摘要/Abstract

摘要： Diamond crystallization was carried out with CH₄N₂S additive in the FeNiCo-C system at pressure 6.0 GPa and temperature ranging from 1290 ℃ to 1300 ℃. The crystallization qualities of the synthetic crystals were characterized by Raman spectra and the Raman peaks located at 1331 cm^-1. Fourier transform infrared (FTIR) results showed that the hydrogen-related absorption peak of the as-grown diamond was at 2920 cm^-1, respectively. Interestingly, A-center nitrogen was observed in the obtained diamond and the characteristic absorption peaks located at 1095 cm^-1 and 1282 cm^-1. Especially, the absorption peak at 1426 cm^-1 attributing to the aggregation B-center nitrogen defect was distinctly found when the CH₄N₂S content reached 0.3 mg in the synthesis system, which was extremely rare in synthetic diamond. Furthermore, optical color centers in the synthesized crystals were investigated by photoluminescence (PL).

关键词: high pressure and high temperature, diamond, crystallization, characteristics

Abstract: Diamond crystallization was carried out with CH₄N₂S additive in the FeNiCo-C system at pressure 6.0 GPa and temperature ranging from 1290 ℃ to 1300 ℃. The crystallization qualities of the synthetic crystals were characterized by Raman spectra and the Raman peaks located at 1331 cm^-1. Fourier transform infrared (FTIR) results showed that the hydrogen-related absorption peak of the as-grown diamond was at 2920 cm^-1, respectively. Interestingly, A-center nitrogen was observed in the obtained diamond and the characteristic absorption peaks located at 1095 cm^-1 and 1282 cm^-1. Especially, the absorption peak at 1426 cm^-1 attributing to the aggregation B-center nitrogen defect was distinctly found when the CH₄N₂S content reached 0.3 mg in the synthesis system, which was extremely rare in synthetic diamond. Furthermore, optical color centers in the synthesized crystals were investigated by photoluminescence (PL).

Key words: high pressure and high temperature, diamond, crystallization, characteristics

中图分类号: (Pressure, density, and temperature)

92.60.hv

81.05.ug (Diamond) 81.10.-h (Methods of crystal growth; physics and chemistry of crystal growth, crystal morphology, and orientation) 61.72.jn (Color centers)

李勇, 谭德斌, 王强, 肖政国, 田昌海, 陈琳. Crystallization and characteristics of {100}-oriented diamond with CH₄N₂S additive under high pressure and high temperature[J]. 中国物理B, 2020, 29(9): 98103-098103.

Yong Li(李勇), Debing Tan(谭德斌), Qiang Wang(王强), Zhengguo Xiao(肖政国), Changhai Tian(田昌海), Lin Chen(陈琳). Crystallization and characteristics of {100}-oriented diamond with CH₄N₂S additive under high pressure and high temperature[J]. Chin. Phys. B, 2020, 29(9): 98103-098103.

参考文献 29

[1]	Guo M M, Li S S, Hu M H, Su T C, Wang J Z, Gao G J, You Y and Nie Y 2020 Chin. Phys. B 29 018101 doi: 10.1088/1674-1056/ab592f
[2]	Li Y, Li Y D, Wang Y, Zhang J, Song M S, She Y C and Chen X Z 2018 Cryst. Eng. Comm. 20 4127 doi: 10.1039/C8CE00786A
[3]	Angerer A, Streltsov K, Astner T, Putz S, Sumiya H, Onoda S, Isoya J, Munro W J, Nemoto K, Schmiedmayer J and Majer J 2018 Nat. Phys. 14 1168 doi: 10.1038/s41567-018-0269-7
[4]	Dutt M V G, Childress L, Jiang L, Togan E, Maze J, Jelezko F, Zibrov A S, Hemmer P R and Lukin M D 2007 Science 316 1312 doi: 10.1126/science.1139831
[5]	Maze J R, Stanwix P L, Hodges J S, Hong S, Taylor J M, Cappellaro P, Jiang L, Zibrov A S, Yacoby A, Walsworth R L and Lukin M D 2008 Nature 455 644 doi: 10.1038/nature07279
[6]	Zhang J F, Yang P Z, Ren Z Y, Zhang J C, Xu S R, Zhang C F, Xu L and Hao Y 2018 Acta Phys. Sin. 67 068101 (in Chinese)
[7]	Xu H, Liu J J, Ye H T, Coathup D J, Khomich A V and Hu X J 2018 Chin. Phys. B 27 096104 doi: 10.1088/1674-1056/27/9/096104
[8]	Hu M H, Bi N, Li S S, Su T C, Hu Q, Jia X P and Ma H A 2015 Chin. Phys. B 24 038101 doi: 10.1088/1674-1056/24/3/038101
[9]	Wang J Z, Li S S, Hu M H, Su T C, Gao G J, Guo M M, You Y and Nie Y 2020 Int. J. Refract. Met. Hard Mater. 87 105150 doi: 10.1016/j.ijrmhm.2019.105150
[10]	Briddon P R and Jones R 1993 Physica B 185 179 doi: 10.1016/0921-4526(93)90235-X
[11]	Salustro S, Ferrari A M, Gentile F S, Denmarais J K and Rérat M 2018 J. Phys. Chem. A 122 594 doi: 10.1021/acs.jpca.7b11551
[12]	Sutherland G B B M, Blackwell D E and Simeral W G 1954 Nature 174 901 doi: 10.1038/174901a0
[13]	Li Y, Jia X P, Hu M H, Yan B M, Zhou Z X, Fang C, Zhang Z F and Ma H A 2012 Int. J. Refract. Met. Hard Mater. 34 27 doi: 10.1016/j.ijrmhm.2012.03.005
[14]	Guo L S, Ma H A, Chen L C, Chen N, Miao X Y, Wang Y, Fang S, Yang Z Q, Fang C and Jia X P 2018 Cryst. Eng. Comm. 20 5457 doi: 10.1039/C8CE00912K
[15]	Li Y, Jia X P, Yan B M, Zhou Z X, Fang C, Zhang Z F, Sun S S and Ma H A 2012 Journal of Crystal Growth 359 49 doi: 10.1016/j.jcrysgro.2012.08.006
[16]	Pal'yanov Y N, Kupriyanov I N, Borzdov Y M, Sokol A G and Khokhryakov A F 2009 Cryst. Growth Des. 9 2922 doi: 10.1021/cg900265c
[17]	Meng Y F, Yan C S, Lai J, Krasnicki S, Shu H Y, Yu T, Liang Q, Mao H K and Hemley Russell J 2008 Proc. Acad. Natl. Sci. USA 105 17620 doi: 10.1073/pnas.0808230105
[18]	Akaishi M, Handa H, Sato Y, Setaka N, Ohsawa T and Fukunaga O 1982 J. Mater. Sci. 17 193 doi: 10.1007/BF00809051
[19]	Fuchs F, Wild C, Schwarz K and Koidl P 1995 Diam. Relat. Mater. 4 652 doi: 10.1016/0925-9635(94)05247-6
[20]	Li Y, Jia X P, Hu M H, Liu X B, Yan B M, Zhou Z X, Zhang Z F and Ma H A 2012 Chin. Phys. B 21 058101 doi: 10.1088/1674-1056/21/5/058101
[21]	Huang G F, Jia X P, Yin J W, Ma H A and Zheng Y J 2013 Int. J. Refractory Metals and Hard Mater 41 517 doi: 10.1016/j.ijrmhm.2013.07.001
[22]	Liu X B, Jia X P, Fang C and Ma H A 2016 Cryst. Eng. Comm. 18 8506 doi: 10.1039/C6CE02034H
[23]	Chen N, Ma H A, Yan B M, Chen L C, Chen L X, Guo L S, Miao X Y, Fang C and Jia X P 2018 Cryst. Growth Des. 18 3870 doi: 10.1021/acs.cgd.8b00145
[24]	Mainwood A 1994 Phys. Rev. B 49 7934 doi: 10.1103/PhysRevB.49.7934
[25]	Li Y, Li S S, She Y C and Guan X M 2017 Journal of Synthetic Crystals 46 778 (in Chinese)
[26]	Lindblom J, Hölsä J, Papunen H and Häkkänen H 2005 American Mineralogist 90 428 doi: 10.2138/am.2005.1681
[27]	Stanwix P L, Pham L M, Maze J R, Le Sage D, Yeung T K, Cappelllaro P, Hemmer P R, Yacoby, Lukin M D and Walsworth R L 2010 Phys. Rev. B 82 201201 doi: 10.1103/PhysRevB.82.201201
[28]	Chen L C, Miao X Y, Ma H A, Guo L S, Wang Z K, Yang Z Q, Fang C and Jia X P 2018 Cryst. Eng. Comm. 20 7164 doi: 10.1039/C8CE01533C
[29]	Rabeau J R, Chin Y L, Prawer S, Jelezko F, Gaebel T and Wrachtrup J 2005 Appl. Phys. Lett. 86 131926 doi: 10.1063/1.1896088

Crystallization and characteristics of {100}-oriented diamond with CH₄N₂S additive under high pressure and high temperature

Crystallization and characteristics of {100}-oriented diamond with CH₄N₂S additive under high pressure and high temperature

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