中国物理B ›› 2016, Vol. 25 ›› Issue (1): 17802-017802.doi: 10.1088/1674-1056/25/1/017802

• CONDENSED MATTER: ELECTRONIC STRUCTURE, ELECTRICAL, MAGNETIC, AND OPTICAL PROPERTIES • 上一篇    下一篇

In-situ SAXS study on PET/ PMMT composites during tensile tests

Wei-Dong Cheng(程伟东), Xiao-Hua Gu(顾晓华), Xue Song(宋雪), Peng Zeng(曾鹏), Zhao-Jun Wu(吴昭君), Xue-Qing Xing(邢雪青), Guang Mo(默广), Zhong-Hua Wu(吴忠华)   

  1. 1. College of Materials Science and Engineering, Qiqihar University, Qiqihar 161006, China;
    2. Department of Practice Teaching and Equipment Management, Qiqihar University, Qiqihar 161006, China;
    3. Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049, China
  • 收稿日期:2015-07-16 修回日期:2015-09-24 出版日期:2016-01-05 发布日期:2016-01-05
  • 通讯作者: Wei-Dong Cheng, Xiao-Hua Gu E-mail:57399942@qq.com;gxh216@163.com
  • 基金资助:
    Project supported by the National Natural Science Foundation of China (Grant Nos. U1232203, U1432104, U1332107, 11305198, and 11405199), the Program for Young Teachers Scientific Research in Qiqihar University, China (Grant No. 2012k-Z02), and the Natural Science Foundation of Heilongjiang Province, China (Grant No. E201259).

In-situ SAXS study on PET/ PMMT composites during tensile tests

Wei-Dong Cheng(程伟东)1, Xiao-Hua Gu(顾晓华)1, Xue Song(宋雪)1, Peng Zeng(曾鹏)1, Zhao-Jun Wu(吴昭君)2, Xue-Qing Xing(邢雪青)3, Guang Mo(默广)3, Zhong-Hua Wu(吴忠华)3   

  1. 1. College of Materials Science and Engineering, Qiqihar University, Qiqihar 161006, China;
    2. Department of Practice Teaching and Equipment Management, Qiqihar University, Qiqihar 161006, China;
    3. Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049, China
  • Received:2015-07-16 Revised:2015-09-24 Online:2016-01-05 Published:2016-01-05
  • Contact: Wei-Dong Cheng, Xiao-Hua Gu E-mail:57399942@qq.com;gxh216@163.com
  • Supported by:
    Project supported by the National Natural Science Foundation of China (Grant Nos. U1232203, U1432104, U1332107, 11305198, and 11405199), the Program for Young Teachers Scientific Research in Qiqihar University, China (Grant No. 2012k-Z02), and the Natural Science Foundation of Heilongjiang Province, China (Grant No. E201259).

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摘要： The nanostructures during the tensile drawing of poly(ethylene terephthalate) (PET)/hexadecyl triphenyl phosphonium bromide montmorillonite (PMMT) nanocomposites were studied by in-situ small angle x-ray scattering. For strain higher than the yield point, the scattering intensity increases dramatically due to the nucleation and growth of nanovoids and crystals. The nanovoids and crystals are significantly dependent on the heating temperature. The effective filling of PMMT in the PET matrix provokes a strong restriction to the long period. The peaks of the long period disappear gradually with the deformation strain increasing from 0% to 34%.

关键词: small angle x-ray scattering, nanostructure, montmorillonite, poly(ethylene terephthalate)

Abstract: The nanostructures during the tensile drawing of poly(ethylene terephthalate) (PET)/hexadecyl triphenyl phosphonium bromide montmorillonite (PMMT) nanocomposites were studied by in-situ small angle x-ray scattering. For strain higher than the yield point, the scattering intensity increases dramatically due to the nucleation and growth of nanovoids and crystals. The nanovoids and crystals are significantly dependent on the heating temperature. The effective filling of PMMT in the PET matrix provokes a strong restriction to the long period. The peaks of the long period disappear gradually with the deformation strain increasing from 0% to 34%.

Key words: small angle x-ray scattering, nanostructure, montmorillonite, poly(ethylene terephthalate)

中图分类号:  (X-ray scattering)

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