Bright blue photoluminescence from a mixed tin and manganese oxide xerogel prepared via sol–hydrothermal–gel process

doi:10.1088/1674-1056/20/12/127801

中国物理B ›› 2011, Vol. 20 ›› Issue (12): 127801-127801.doi: 10.1088/1674-1056/20/12/127801

Bright blue photoluminescence from a mixed tin and manganese oxide xerogel prepared via sol–hydrothermal–gel process

周维列¹, 向霞², 李志杰², 刘春明², 祖小涛², 程晓峰³, 贺少勃³, 袁晓东³, 郑万国³

(1)Advanced Materials Research Institute, University of New Orleans, New Orleans, Louisiana 70148, USA; (2)Department of Applied Physics, University of Electronic Science and Technology of China, Chengdu 610054, China; (3)Research Centre of Laser Fusion, China Academy of Engineering Physics, Mianyang 621900, China

收稿日期:2011-06-08 修回日期:2011-07-12 出版日期:2011-12-15 发布日期:2011-12-15
基金资助:
Project supported by the National Natural Science Foundation of China (Grant No. 10904008), Joint Funds of the National Natural Science Foundation of China (Grant No. 11076008), and the Young Scientists Foundation of Sichuan Province of China (Grant No. 2010JQ0006).

Bright blue photoluminescence from a mixed tin and manganese oxide xerogel prepared via sol–hydrothermal–gel process

Xiang Xia(向霞)^a)^†, Cheng Xiao-Feng(程晓峰)^b), He Shao-Bo(贺少勃)^b), Yuan Xiao-Dong(袁晓东)^b), Zheng Wan-Guo(郑万国)^b), Li Zhi-Jie(李志杰)^a),Liu Chun-Ming(刘春明)^a), Zhou Wei-Lie(周维列)^c), and Zu Xiao-Tao (祖小涛)^a)

^a Department of Applied Physics, University of Electronic Science and Technology of China, Chengdu 610054, China; ^b Research Centre of Laser Fusion, China Academy of Engineering Physics, Mianyang 621900, China; ^cAdvanced Materials Research Institute, University of New Orleans, New Orleans, Louisiana 70148, USA

Received:2011-06-08 Revised:2011-07-12 Online:2011-12-15 Published:2011-12-15
Supported by:
Project supported by the National Natural Science Foundation of China (Grant No. 10904008), Joint Funds of the National Natural Science Foundation of China (Grant No. 11076008), and the Young Scientists Foundation of Sichuan Province of China (Grant No. 2010JQ0006).

摘要/Abstract

摘要： A new blue photoluminescent material, a mixed tin and manganese oxide xerogel, is prepared via sol-hydrothermal-gel process assisted by citric acid. The composition xerogel exhibits strong blue emission at room temperature, with an emission maximum at 434 nm under short (234 nm) or long-wavelength (343 nm) ultraviolet excitation. The photoluminescent excitation spectrum of the mixed tin and manganese oxide xerogel, monitored at an intensity maximum wavelength of 434 nm of the emission, consists of two excitation peaks at 234 nm and 343 nm. With heat treatment temperature increasing from 110 ℃ to 200 ℃, the blue emission intensity increases remarkably, whereas it is almost completely quenched after being treated at 300 ℃. The carbon impurities in the mixed tin and manganese oxide xerogel, confirmed by Fourier transform infrared spectroscopy and X-ray photoelectron spectroscopy, should be responsible for the bright blue photoluminescence.

关键词: xerogel, photoluminescence, hydrothermal, sol-gel

Abstract: A new blue photoluminescent material, a mixed tin and manganese oxide xerogel, is prepared via sol-hydrothermal-gel process assisted by citric acid. The composition xerogel exhibits strong blue emission at room temperature, with an emission maximum at 434 nm under short (234 nm) or long-wavelength (343 nm) ultraviolet excitation. The photoluminescent excitation spectrum of the mixed tin and manganese oxide xerogel, monitored at an intensity maximum wavelength of 434 nm of the emission, consists of two excitation peaks at 234 nm and 343 nm. With heat treatment temperature increasing from 110 ℃ to 200 ℃, the blue emission intensity increases remarkably, whereas it is almost completely quenched after being treated at 300 ℃. The carbon impurities in the mixed tin and manganese oxide xerogel, confirmed by Fourier transform infrared spectroscopy and X-ray photoelectron spectroscopy, should be responsible for the bright blue photoluminescence.

Key words: xerogel, photoluminescence, hydrothermal, sol-gel

中图分类号: (Photoluminescence, properties and materials)

78.55.-m

78.66.Sq (Composite materials)

向霞, 程晓峰, 贺少勃, 袁晓东, 郑万国, 李志杰, 刘春明, 周维列, 祖小涛. Bright blue photoluminescence from a mixed tin and manganese oxide xerogel prepared via sol–hydrothermal–gel process[J]. 中国物理B, 2011, 20(12): 127801-127801.

Xiang Xia(向霞), Cheng Xiao-Feng(程晓峰), He Shao-Bo(贺少勃), Yuan Xiao-Dong(袁晓东), Zheng Wan-Guo(郑万国), Li Zhi-Jie(李志杰), Liu Chun-Ming(刘春明), Zhou Wei-Lie(周维列), and Zu Xiao-Tao (祖小涛) . Bright blue photoluminescence from a mixed tin and manganese oxide xerogel prepared via sol–hydrothermal–gel process[J]. Chin. Phys. B, 2011, 20(12): 127801-127801.

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Bright blue photoluminescence from a mixed tin and manganese oxide xerogel prepared via sol–hydrothermal–gel process

Bright blue photoluminescence from a mixed tin and manganese oxide xerogel prepared via sol–hydrothermal–gel process

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